tetraphenylphosphonium oxotetrachlororhenate(V)

Base Information

Chemical Name:tetraphenylphosphonium oxotetrachlororhenate(V)
CAS No.:62776-43-6
Molecular Formula:C₂₄H₂₀P*Cl₄ORe
Molecular Weight:683.415
Hs Code.:

Synonyms:tetraphenylphosphonium oxotetrachlororhenate(V)

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Chemical Property of tetraphenylphosphonium oxotetrachlororhenate(V)

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Technology Process of tetraphenylphosphonium oxotetrachlororhenate(V)

There total 1 articles about tetraphenylphosphonium oxotetrachlororhenate(V) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 10466-65-6
potassium perrhenate

: 2001-45-8
tetraphenyl phosphonium chloride

: 62776-43-6
tetraphenylphosphonium oxotetrachlororhenate(V)

Guidance literature:: In hydrogenchloride; acetic acid; (N2); KReO4 was dissolved in acetic acid/HCl; Ph4PCl was added; pptn. by vigorous shaking; supernatant liquid decanted off; ppt. washed with acetic acid-HCl and petroleum ether and dried under N2; elem. anal.;

Reference yield: 73.0%

: 62776-43-6
tetraphenylphosphonium oxotetrachlororhenate(V)

: 502470-00-0
N-[N-3(diphenylphosphinopropionyl)glycyl]cysteine methyl ester

: ReCl₃OP(C₆H₅)2C₂H₄CONHCH₂CONHCH(CH₂S)COOCH₃^(1-)*P(C₆H₅)4⁽¹⁺⁾=P(C₆H₅)4ReCl₃OP(C₆H₅)2C₂H₄CONHCH₂CONHCHCH₂SCO₂CH₃

Guidance literature:: In not given; cysteine-compound was dissolved in abs. ethanol or CH3CN, a soln. of complex in the same solvent was added at room temp., the suspn. was stirredunder Ar for 4 h; filtered, washed with abs. ethanol; elem. anal.;
DOI:10.1021/ic025859r

Reference yield: 54.0%

: 60-29-7,927820-24-4
diethyl ether

: 62776-43-6
tetraphenylphosphonium oxotetrachlororhenate(V)

: 75-09-2
dichloromethane

: 157432-87-6,288302-11-4,288302-12-5,60705-62-6
5,11,17,23-tetra-t-butyl-25,26,27,28-tetrahydroxycalix-4-arene

: (Ph₄P)ReClO[p-tBu-calixarene-(O)4]*CH₂Cl₂*0.5(C₂H₅)2O

Guidance literature:: With BuLi; In tetrahydrofuran; soln. of p-tBu-calix(4)arene-(OH)4 in THF was treated with BuLi; then reacted with (Ph4P)(ReOCl4);
DOI:10.1002/anie.200351530