carbonic acid allyl ester 4-{2-allyloxycarbonylamino-2-[4-(4-methyl-2-oxo-2H-chromen-7-ylcarbamoyloxymethyl)-phenylcarbamoyl]-ethyl}-phenyl ester

Base Information

Chemical Name:carbonic acid allyl ester 4-{2-allyloxycarbonylamino-2-[4-(4-methyl-2-oxo-2H-chromen-7-ylcarbamoyloxymethyl)-phenylcarbamoyl]-ethyl}-phenyl ester
CAS No.:728916-21-0
Molecular Formula:C₃₅H₃₃N₃O₁₀
Molecular Weight:655.661
Hs Code.:

carbonic acid allyl ester 4-{2-allyloxycarbonylamino-2-[4-(4-methyl-2-oxo-2<i>H</i>-chromen-7-ylcarbamoyloxymethyl)-phenylcarbamoyl]-ethyl}-phenyl ester

Synonyms:carbonic acid allyl ester 4-{2-allyloxycarbonylamino-2-[4-(4-methyl-2-oxo-2H-chromen-7-ylcarbamoyloxymethyl)-phenylcarbamoyl]-ethyl}-phenyl ester

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Chemical Property of carbonic acid allyl ester 4-{2-allyloxycarbonylamino-2-[4-(4-methyl-2-oxo-2H-chromen-7-ylcarbamoyloxymethyl)-phenylcarbamoyl]-ethyl}-phenyl ester

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Technology Process of carbonic acid allyl ester 4-{2-allyloxycarbonylamino-2-[4-(4-methyl-2-oxo-2H-chromen-7-ylcarbamoyloxymethyl)-phenylcarbamoyl]-ethyl}-phenyl ester

There total 3 articles about carbonic acid allyl ester 4-{2-allyloxycarbonylamino-2-[4-(4-methyl-2-oxo-2H-chromen-7-ylcarbamoyloxymethyl)-phenylcarbamoyl]-ethyl}-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 7-isocyanato-4-methylcoumarine

: 728916-20-9
Carbonic acid allyl ester 4-[(S)-2-allyloxycarbonylamino-2-(4-hydroxymethyl-phenylcarbamoyl)-ethyl]-phenyl ester

: 728916-21-0
carbonic acid allyl ester 4-{2-allyloxycarbonylamino-2-[4-(4-methyl-2-oxo-2H-chromen-7-ylcarbamoyloxymethyl)-phenylcarbamoyl]-ethyl}-phenyl ester

Guidance literature:: In toluene; for 2h; Heating;
DOI:10.1016/j.bmcl.2004.04.041 DOI:10.1016/j.bmc.2005.08.015

Reference yield:

: 623-04-1
4-aminobenzenemethanol

: 728916-21-0
carbonic acid allyl ester 4-{2-allyloxycarbonylamino-2-[4-(4-methyl-2-oxo-2H-chromen-7-ylcarbamoyloxymethyl)-phenylcarbamoyl]-ethyl}-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / EDCI; HOBt / tetrahydrofuran / 12 h / 20 °C

2: 98 percent / toluene / 2 h / Heating

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; toluene;
DOI:10.1016/j.bmc.2005.08.015

Reference yield:

: 104669-68-3
N,O-bis-allyloxycarbonyl-L-tyrosine

: 728916-21-0
carbonic acid allyl ester 4-{2-allyloxycarbonylamino-2-[4-(4-methyl-2-oxo-2H-chromen-7-ylcarbamoyloxymethyl)-phenylcarbamoyl]-ethyl}-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / EDCI; HOBt / tetrahydrofuran / 12 h / 20 °C

2: 98 percent / toluene / 2 h / Heating

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; toluene;
DOI:10.1016/j.bmc.2005.08.015