tetraethylammonium pentachloro(pyridine)iridate(IV)

Base Information

Chemical Name:tetraethylammonium pentachloro(pyridine)iridate(IV)
CAS No.:118773-91-4
Molecular Formula:C₅H₅Cl₅IrN*C₈H₂₀N
Molecular Weight:578.84
Hs Code.:

Synonyms:tetraethylammonium pentachloro(pyridine)iridate(IV)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetraethylammonium pentachloro(pyridine)iridate(IV)

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of tetraethylammonium pentachloro(pyridine)iridate(IV)

There total 1 articles about tetraethylammonium pentachloro(pyridine)iridate(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39210-66-7,53199-34-1,94534-90-4
trans-{Ir(pyridine)2Cl₄}

: 56-34-8
tetraethylammonium chloride

: 118773-91-4
tetraethylammonium pentachloro(pyridine)iridate(IV)

: 628-13-7
pyridine hydrochloride

Guidance literature:: With hydrogen chloride; In dichloromethane; excess NEt4Cl, HCl bubbled for 1 h into the soln., purged with N2; evapn. to dryness, washed with water, dried in vac.; elem. anal.;

Reference yield: 20.0%

: 118773-91-4
tetraethylammonium pentachloro(pyridine)iridate(IV)

: 50-81-7,98966-42-8
ascorbic acid

: 118773-77-6
tetraethylammonium pentachloro(triphenylphosphine)iridate(IV)

: 628-13-7
pyridine hydrochloride

Guidance literature:: With P(C₆H₅)3; chlorine; HCl; In ethanol; dichloromethane; Ir-compd. dissolved in warm ethanol, dropwise addn. of ascorbic acid in ethanol, addn. of ligand in CH2Cl2, refluxed for 1 h, ethanol evapd. in vac., dissolved in CH2Cl2, oxidised with chlorine, saturated with HCl, after 1 h purged with nitrogen; partioned with water, organic phase separated and dried over Na2SO4, reduced in vac., addn. of diethyl ether, left at -10°C, liquid decanted off, dried in vac.; elem. anal.;

Reference yield: 20.0%

: 118773-91-4
tetraethylammonium pentachloro(pyridine)iridate(IV)

: 75-18-3
dimethylsulfide

: 50-81-7,98966-42-8
ascorbic acid

: 118773-83-4
tetraethylammonium pentachloro(dimethylsulphide)iridate(IV)

: 628-13-7
pyridine hydrochloride

Guidance literature:: With HCl; chlorine; In ethanol; dichloromethane; Ir-compd. dissolved in warm ethanol, dropwise addn. of ascorbic acid in ethanol, addn. of ligand in CH2Cl2, refluxed for 1 h, ethanol evapd. in vac., dissolved in CH2Cl2, oxidised with chlorine, saturated with HCl, after 1 h purged with nitrogen; partioned with water, organic phase separated and dried over Na2SO4, reduced in vac., addn. of diethyl ether, left at -10°C, liquid decanted off, dried in vac.; elem. anal.;