3,5-dimethoxyphenyl diethylcarbamate

Base Information

• Chemical Name: 3,5-dimethoxyphenyl diethylcarbamate
• CAS No.: 1025324-83-7
• Molecular Formula: C₁₃H₁₉NO₄
• Molecular Weight: 253.298
• Mol file: 1025324-83-7.mol

Synonyms:3,5-dimethoxyphenyl diethylcarbamate

Chemical Property of 3,5-dimethoxyphenyl diethylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,5-dimethoxyphenyl diethylcarbamate

There total 1 articles about 3,5-dimethoxyphenyl diethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

3,5-dimethoxyphenol (500-99-2) + N,N-diethylcarbamyl chloride (88-10-8) → 3,5-dimethoxyphenyl diethylcarbamate (1025324-83-7)

Guidance literature:

With potassium carbonate; In acetonitrile; for 12h; Heating;

DOI:10.1002/ejoc.200701116

Reference yield: 97.0%

3,5-dimethoxyphenyl diethylcarbamate (1025324-83-7) → 2-(diethylcarbamoyloxy)-3,5-dimethoxyphenylboronic acid (1135822-19-3)

Guidance literature:

3,5-dimethoxyphenyl diethylcarbamate; With Triisopropyl borate; lithium diisopropyl amide; In tetrahydrofuran; at -78 - 0 ℃;

In water;

DOI:10.1002/ejoc.200701116

Reference yield: 86.0%

3,5-dimethoxyphenyl diethylcarbamate (1025324-83-7)

Guidance literature:

3,5-dimethoxyphenyl diethylcarbamate; With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In tetrahydrofuran; cyclohexane; at -78 ℃; for 0.166667h;

With iodine; In tetrahydrofuran; cyclohexane; at -78 ℃;

DOI:10.1002/ejoc.200701116

upstream raw materials:

3,5-dimethoxyphenol

N,N-diethylcarbamyl chloride

Downstream raw materials:

2-but-2-ynoyl-3,5-dimethoxyphenyl diethylcarbamate

2-(diethylcarbamoyloxy)-3,5-dimethoxyphenylboronic acid

3,5-dimethoxy-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl diethylcarbamate

C₂₄H₃₆N₂O₄Si