3,5-dimethoxy-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl diethylcarbamate

Base Information

Chemical Name:3,5-dimethoxy-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl diethylcarbamate
CAS No.:1032189-97-1
Molecular Formula:C₁₉H₃₀BNO₆
Molecular Weight:379.261
Hs Code.:

Synonyms:3,5-dimethoxy-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl diethylcarbamate

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Chemical Property of 3,5-dimethoxy-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl diethylcarbamate

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Technology Process of 3,5-dimethoxy-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl diethylcarbamate

There total 2 articles about 3,5-dimethoxy-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl diethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 1135822-19-3
2-(diethylcarbamoyloxy)-3,5-dimethoxyphenylboronic acid

: 1032189-97-1
3,5-dimethoxy-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl diethylcarbamate

Guidance literature:: In ethyl acetate;
DOI:10.1002/ejoc.200701116

Reference yield:

: 1025324-83-7
3,5-dimethoxyphenyl diethylcarbamate

: 1032189-97-1
3,5-dimethoxy-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl diethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C

1.2: 0.5 h / -78 °C

2.1: hydrogenchloride / water / 0 °C / pH < 5

With hydrogenchloride; lithium diisopropyl amide; In tetrahydrofuran; water;
DOI:10.3987/COM-12-S(N)131

Reference yield: 99.0%

: 1032189-97-1
3,5-dimethoxy-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl diethylcarbamate

: 19524-06-2
4-bromopyridine hydrochloride

: 1032189-92-6
3,5-dimethoxy-2-(pyridin-4-yl)phenyl diethylcarbamate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,2-dimethoxyethane; water; at 90 ℃; for 20h;
DOI:10.1002/ejoc.200701116