C₂₃H₂₆BF₃O₅

Base Information

Chemical Name:C₂₃H₂₆BF₃O₅
CAS No.:1364267-33-3
Molecular Formula:C₂₃H₂₆BF₃O₅
Molecular Weight:450.263
Hs Code.:

C<sub>23</sub>H<sub>26</sub>BF<sub>3</sub>O<sub>5</sub>

Synonyms:C₂₃H₂₆BF₃O₅

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Chemical Property of C₂₃H₂₆BF₃O₅

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Technology Process of C₂₃H₂₆BF₃O₅

There total 3 articles about C₂₃H₂₆BF₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.6%

: 1364267-24-2
(R)-methyl 4-bromo-2-(1-(2-(trifluoromethyl)phenyl)ethoxy)benzoate

: 73183-34-3
bis(pinacol)diborane

: 1364267-33-3
C₂₃H₂₆BF₃O₅

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,4-dioxane; at 90 ℃; Inert atmosphere;

Reference yield:

: 1666-28-0
4-bromosalicylic acid

: 1364267-33-3
C₂₃H₂₆BF₃O₅

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 24 h / 80 °C

2: di-tert-butyl-diazodicarboxylate; triphenylphosphine / dichloromethane / 0 - 20 °C

3: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / N,N-dimethyl-formamide / 1.5 h / 100 °C / Microwave irradiation

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; di-tert-butyl-diazodicarboxylate; sulfuric acid; potassium acetate; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide; 2: Mitsunobu reaction;
DOI:10.1021/jm201683b

Reference yield:

: 22717-56-2
4-bromo-2-Hydroxybenzoic Acid Methylester

: 1364267-33-3
C₂₃H₂₆BF₃O₅

Guidance literature:: Multi-step reaction with 2 steps

1: di-tert-butyl-diazodicarboxylate; triphenylphosphine / dichloromethane / 0 - 20 °C

2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / N,N-dimethyl-formamide / 1.5 h / 100 °C / Microwave irradiation

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; di-tert-butyl-diazodicarboxylate; potassium acetate; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide; 1: Mitsunobu reaction;
DOI:10.1021/jm201683b