tert-butyl 1-(4-(5-amino-6-oxo-3-phenyl-1,6-dihydropyridin-2-yl)phenyl)cyclobutylcarbamate

Base Information

Chemical Name:tert-butyl 1-(4-(5-amino-6-oxo-3-phenyl-1,6-dihydropyridin-2-yl)phenyl)cyclobutylcarbamate
CAS No.:1313440-28-6
Molecular Formula:C₂₆H₂₉N₃O₃
Molecular Weight:431.535
Hs Code.:

Synonyms:tert-butyl 1-(4-(5-amino-6-oxo-3-phenyl-1,6-dihydropyridin-2-yl)phenyl)cyclobutylcarbamate

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Chemical Property of tert-butyl 1-(4-(5-amino-6-oxo-3-phenyl-1,6-dihydropyridin-2-yl)phenyl)cyclobutylcarbamate

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Technology Process of tert-butyl 1-(4-(5-amino-6-oxo-3-phenyl-1,6-dihydropyridin-2-yl)phenyl)cyclobutylcarbamate

There total 3 articles about tert-butyl 1-(4-(5-amino-6-oxo-3-phenyl-1,6-dihydropyridin-2-yl)phenyl)cyclobutylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 1313440-27-5
tert-butyl (1-(4-(5-carbamoyl-6-hydroxy-3-phenylpyridin-2-yl)phenyl)cyclobutyl)carbamate

: 1313440-28-6
tert-butyl (1-(4-(5-amino-6-hydroxy-3-phenylpyridin-2-yl)phenyl)cyclobutyl)carbamate

Guidance literature:: With bromine; sodium hydroxide; In water; at 0 - 65 ℃; for 24h;

Reference yield:

: 1313440-25-3
(E)-tert-butyl (1-(4-(3-(dimethylamino)-2-phenylacryloyl)phenyl)cyclobutyl)carbamate

: 1313440-28-6
tert-butyl (1-(4-(5-amino-6-hydroxy-3-phenylpyridin-2-yl)phenyl)cyclobutyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; methanol / 16 h / 0 - 40 °C

2.1: sodium hydroxide; dihydrogen peroxide / ethanol; water / 16 h / 20 - 50 °C

2.2: 0 °C / pH 4

3.1: sodium hydroxide; bromine / water / 24 h / 0 - 65 °C

With dihydrogen peroxide; bromine; sodium hydride; sodium hydroxide; In methanol; ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 1313440-26-4
tert-butyl (1-(4-(5-cyano-6-hydroxy-3-phenylpyridin-2-yl)phenyl)cyclobutyl)carbamate

: 1313440-28-6
tert-butyl (1-(4-(5-amino-6-hydroxy-3-phenylpyridin-2-yl)phenyl)cyclobutyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide; dihydrogen peroxide / ethanol; water / 16 h / 20 - 50 °C

1.2: 0 °C / pH 4

2.1: sodium hydroxide; bromine / water / 24 h / 0 - 65 °C

With dihydrogen peroxide; bromine; sodium hydroxide; In ethanol; water;