2-(2-azidophenyl)-N-tert-butyl-2-(3-(3-methoxyphenyl)prop-2-ynyloxy)acetamide

Base Information

Chemical Name:2-(2-azidophenyl)-N-tert-butyl-2-(3-(3-methoxyphenyl)prop-2-ynyloxy)acetamide
CAS No.:1592942-63-6
Molecular Formula:C₂₂H₂₄N₄O₃
Molecular Weight:392.458
Hs Code.:

Synonyms:2-(2-azidophenyl)-N-tert-butyl-2-(3-(3-methoxyphenyl)prop-2-ynyloxy)acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2-azidophenyl)-N-tert-butyl-2-(3-(3-methoxyphenyl)prop-2-ynyloxy)acetamide

Chemical Property:

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Technology Process of 2-(2-azidophenyl)-N-tert-butyl-2-(3-(3-methoxyphenyl)prop-2-ynyloxy)acetamide

There total 3 articles about 2-(2-azidophenyl)-N-tert-butyl-2-(3-(3-methoxyphenyl)prop-2-ynyloxy)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-(3-bromoprop-1-yn-1-yl)-3-methoxybenzene

: 1193490-24-2
1-(2-azidophenyl)-2-(tert-butylamino)-2-oxoethyl acetate

: 1592942-63-6
2-(2-azidophenyl)-N-tert-butyl-2-(3-(3-methoxyphenyl)prop-2-ynyloxy)acetamide

Guidance literature:: With tetrabutylammomium bromide; water; sodium hydroxide; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol500813p

Reference yield:

: 20615-76-3
2-azidobenzyl alcohol

: 1592942-63-6
2-(2-azidophenyl)-N-tert-butyl-2-(3-(3-methoxyphenyl)prop-2-ynyloxy)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

2: dichloromethane / 48 h / 20 °C / Inert atmosphere

3: tetrabutylammomium bromide; sodium hydroxide; water / dichloromethane / 20 °C / Inert atmosphere

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; tetrabutylammomium bromide; water; sodium hydroxide; In dichloromethane; 2: |Passerini Condensation;
DOI:10.1021/ol500813p

Reference yield:

: 16714-25-3
2-azidobenzaldehyde

: 1592942-63-6
2-(2-azidophenyl)-N-tert-butyl-2-(3-(3-methoxyphenyl)prop-2-ynyloxy)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 48 h / 20 °C / Inert atmosphere

2: tetrabutylammomium bromide; sodium hydroxide; water / dichloromethane / 20 °C / Inert atmosphere

With tetrabutylammomium bromide; water; sodium hydroxide; In dichloromethane; 1: |Passerini Condensation;
DOI:10.1021/ol500813p