4-nitrophenyl O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-2,3-di-O-benzoyl-β-D-xylopyranoside

Base Information

Chemical Name:4-nitrophenyl O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-2,3-di-O-benzoyl-β-D-xylopyranoside
CAS No.:173468-19-4
Molecular Formula:C₅₁H₄₁NO₁₆
Molecular Weight:923.884
Hs Code.:

Synonyms:4-nitrophenyl O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-2,3-di-O-benzoyl-β-D-xylopyranoside

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Chemical Property of 4-nitrophenyl O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-2,3-di-O-benzoyl-β-D-xylopyranoside

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Technology Process of 4-nitrophenyl O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-2,3-di-O-benzoyl-β-D-xylopyranoside

There total 3 articles about 4-nitrophenyl O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-2,3-di-O-benzoyl-β-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 173468-17-2
O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-2,3-di-O-benzoyl-α-D-xylopyranosyl bromide

: 173468-19-4
4-nitrophenyl O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-2,3-di-O-benzoyl-β-D-xylopyranoside

Guidance literature:: With potassium carbonate; In acetone; Ambient temperature;
DOI:10.1016/0008-6215(95)00214-E

Reference yield:

: 98-88-4
benzoyl chloride

: 173468-19-4
4-nitrophenyl O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-2,3-di-O-benzoyl-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 51 percent / pyridine / 5 h / Ambient temperature

2: 86 percent / HBr, AcOH / 1,2-dichloro-ethane / 0.5 h / Ambient temperature

3: 68 percent / K₂CO₃ / acetone / Ambient temperature

With pyridine; hydrogen bromide; potassium carbonate; acetic acid; In 1,2-dichloro-ethane; acetone;
DOI:10.1016/0008-6215(95)00214-E

Reference yield:

: 173468-16-1
O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-1,2,3-tri-O-benzoyl-β-D-xylopyranose

: 173468-19-4
4-nitrophenyl O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-2,3-di-O-benzoyl-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / HBr, AcOH / 1,2-dichloro-ethane / 0.5 h / Ambient temperature

2: 68 percent / K₂CO₃ / acetone / Ambient temperature

With hydrogen bromide; potassium carbonate; acetic acid; In 1,2-dichloro-ethane; acetone;
DOI:10.1016/0008-6215(95)00214-E