N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-isopropylcyclopropanecarboxamide

Base Information

Chemical Name:N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-isopropylcyclopropanecarboxamide
CAS No.:1346641-03-9
Molecular Formula:C₁₄H₁₂F₄N₂O
Molecular Weight:300.256
Hs Code.:

Synonyms:N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-isopropylcyclopropanecarboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-isopropylcyclopropanecarboxamide

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Technology Process of N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-isopropylcyclopropanecarboxamide

There total 4 articles about N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-isopropylcyclopropanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1346641-17-5
C₁₁H₂₀O₂

: 1346641-03-9
N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-isopropylcyclopropanecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; water / 1,4-dioxane / 20 °C

2: oxalyl dichloride / dichloromethane / 0 - 20 °C / Inert atmosphere

3: toluene / 12 h / Reflux

With hydrogenchloride; oxalyl dichloride; water; In 1,4-dioxane; dichloromethane; toluene;
DOI:10.1021/ja207607s

Reference yield:

: 773-82-0
Pentafluorobenzonitrile

: 1346641-03-9
N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-isopropylcyclopropanecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: ammonia / water; ethyl acetate / 6 h / 20 °C

2: toluene / 12 h / Reflux

With ammonia; In water; ethyl acetate; toluene;
DOI:10.1021/ja207607s

Reference yield:

: 104131-92-2
1-(1-Methylethyl)cyclopropancarbonsaeure

: 1346641-03-9
N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-isopropylcyclopropanecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / dichloromethane / 0 - 20 °C / Inert atmosphere

2: toluene / 12 h / Reflux

With oxalyl dichloride; In dichloromethane; toluene;
DOI:10.1021/ja207607s