4-(4-Chloro-benzyl)-9-methylsulfanyl-6,7-dihydro-4H-imidazo[1,2-a]purine

Base Information

Chemical Name:4-(4-Chloro-benzyl)-9-methylsulfanyl-6,7-dihydro-4H-imidazo[1,2-a]purine
CAS No.:75217-20-8
Molecular Formula:C₁₅H₁₄ClN₅S
Molecular Weight:331.829
Hs Code.:

Synonyms:4-(4-Chloro-benzyl)-9-methylsulfanyl-6,7-dihydro-4H-imidazo[1,2-a]purine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(4-Chloro-benzyl)-9-methylsulfanyl-6,7-dihydro-4H-imidazo[1,2-a]purine

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Technology Process of 4-(4-Chloro-benzyl)-9-methylsulfanyl-6,7-dihydro-4H-imidazo[1,2-a]purine

There total 6 articles about 4-(4-Chloro-benzyl)-9-methylsulfanyl-6,7-dihydro-4H-imidazo[1,2-a]purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 75185-06-7
4-<(4-chlorophenyl)methyl>-6,7-dihydro-3H-imidazo<1,2-a>purine-9(4H)-thione

: 74-88-4
methyl iodide

: 75217-20-8
4-(4-Chloro-benzyl)-9-methylsulfanyl-6,7-dihydro-4H-imidazo[1,2-a]purine

Guidance literature:: With sodium hydroxide; for 16h; Ambient temperature;
DOI:10.1021/jm00185a008

Reference yield:

: 104-86-9
4-chlorobenzylamine

: 75217-20-8
4-(4-Chloro-benzyl)-9-methylsulfanyl-6,7-dihydro-4H-imidazo[1,2-a]purine

Guidance literature:: Multi-step reaction with 5 steps

1: ethanol / 2 h / Heating

2: EtONa / ethanol / 3 h / Heating

3: 93 percent / 0.2 h

4: 52 percent / P₂S₅ / pyridine / 5 h / Heating

5: 82 percent / 0.1 N NaOH / 16 h / Ambient temperature

With sodium hydroxide; tetraphosphorus decasulfide; sodium ethanolate; In pyridine; ethanol;
DOI:10.1021/jm00185a008

Reference yield:

: 68020-39-3
2-<<(4-chlorophenyl)methyl>amino>-2-imidazoline

: 75217-20-8
4-(4-Chloro-benzyl)-9-methylsulfanyl-6,7-dihydro-4H-imidazo[1,2-a]purine

Guidance literature:: Multi-step reaction with 4 steps

1: EtONa / ethanol / 3 h / Heating

2: 93 percent / 0.2 h

3: 52 percent / P₂S₅ / pyridine / 5 h / Heating

4: 82 percent / 0.1 N NaOH / 16 h / Ambient temperature

With sodium hydroxide; tetraphosphorus decasulfide; sodium ethanolate; In pyridine; ethanol;
DOI:10.1021/jm00185a008