4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoro-undecanoic acid methyl-[4-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-ylsulfanyl)-phenyl]-amide

Base Information

Chemical Name:4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoro-undecanoic acid methyl-[4-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-ylsulfanyl)-phenyl]-amide
CAS No.:724733-06-6
Molecular Formula:C₂₄H₂₂F₁₇NO₆S
Molecular Weight:775.481
Hs Code.:

4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoro-undecanoic acid methyl-[4-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-ylsulfanyl)-phenyl]-amide

Synonyms:4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoro-undecanoic acid methyl-[4-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-ylsulfanyl)-phenyl]-amide

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Chemical Property of 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoro-undecanoic acid methyl-[4-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-ylsulfanyl)-phenyl]-amide

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Technology Process of 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoro-undecanoic acid methyl-[4-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-ylsulfanyl)-phenyl]-amide

There total 5 articles about 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoro-undecanoic acid methyl-[4-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-ylsulfanyl)-phenyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: Acetic acid (2S,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-{4-[(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecanoyl)-methyl-amino]-phenylsulfanyl}-tetrahydro-pyran-3-yl ester

: 724733-06-6
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoro-undecanoic acid methyl-[4-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-ylsulfanyl)-phenyl]-amide

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 5h;
DOI:10.1016/j.tetlet.2004.04.116

Reference yield:

: 724733-04-4
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecanoic acid (4-mercapto-phenyl)-methyl-amide

: 724733-06-6
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoro-undecanoic acid methyl-[4-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-ylsulfanyl)-phenyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / Na₂CO₃ / H₂O; ethyl acetate / 2 h / 20 °C

2: 100 percent / CH₃ONa / methanol / 5 h / 20 °C

With sodium methylate; sodium carbonate; In methanol; water; ethyl acetate;
DOI:10.1016/j.tetlet.2004.04.116

Reference yield:

: 724733-03-3
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecanoic acid (4-methanesulfinyl-phenyl)-methyl-amide

: 724733-06-6
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoro-undecanoic acid methyl-[4-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-ylsulfanyl)-phenyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic anhydride / 0.83 h / 40 °C

1.2: 75 percent / NaOH / H₂O / 2 h / 0 °C

2.1: 100 percent / Na₂CO₃ / H₂O; ethyl acetate / 2 h / 20 °C

3.1: 100 percent / CH₃ONa / methanol / 5 h / 20 °C

With sodium methylate; sodium carbonate; trifluoroacetic anhydride; In methanol; water; ethyl acetate;
DOI:10.1016/j.tetlet.2004.04.116