2,2,4,4-tetramethyl-3-(3-methoxy)benzylidene-1,5-dioxa-2,4-disilacycloheptane

Base Information

Chemical Name:2,2,4,4-tetramethyl-3-(3-methoxy)benzylidene-1,5-dioxa-2,4-disilacycloheptane
CAS No.:1177254-34-0
Molecular Formula:C₁₅H₂₄O₃Si₂
Molecular Weight:308.525
Hs Code.:

Synonyms:2,2,4,4-tetramethyl-3-(3-methoxy)benzylidene-1,5-dioxa-2,4-disilacycloheptane

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Chemical Property of 2,2,4,4-tetramethyl-3-(3-methoxy)benzylidene-1,5-dioxa-2,4-disilacycloheptane

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Technology Process of 2,2,4,4-tetramethyl-3-(3-methoxy)benzylidene-1,5-dioxa-2,4-disilacycloheptane

There total 1 articles about 2,2,4,4-tetramethyl-3-(3-methoxy)benzylidene-1,5-dioxa-2,4-disilacycloheptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 766-85-8
3-methoxy-1-iodobenzene

: 824985-52-6
2,2,4,4-tetramethyl-3-methylene-1,5-dioxa-2,4-disilacycloheptane

: 1177254-34-0
2,2,4,4-tetramethyl-3-(3-methoxy)benzylidene-1,5-dioxa-2,4-disilacycloheptane

Guidance literature:: With palladium diacetate; silver nitrate; triethylamine; triphenylphosphine; In acetonitrile; at 60 ℃; for 1h;
DOI:10.1016/j.tet.2009.01.113

Reference yield: 92.0%

: 13329-40-3
4-Iodoacetophenone

: 1177254-34-0
2,2,4,4-tetramethyl-3-(3-methoxy)benzylidene-1,5-dioxa-2,4-disilacycloheptane

: 1177254-42-0
(E)-4-acetyl-3'-methoxystilbene

Guidance literature:: With bis(η3-allyl-μ-chloropalladium(II)); tetrabutyl ammonium fluoride; In tetrahydrofuran; at 65 ℃; for 1h; stereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2009.01.113