(1-benzyl-4,6-dimethoxyindol-2-yl)-phenylmethanone O-2,4-dinitrophenyloxime

Base Information

Chemical Name:(1-benzyl-4,6-dimethoxyindol-2-yl)-phenylmethanone O-2,4-dinitrophenyloxime
CAS No.:945620-15-5
Molecular Formula:C₃₀H₂₄N₄O₇
Molecular Weight:552.543
Hs Code.:

Synonyms:(1-benzyl-4,6-dimethoxyindol-2-yl)-phenylmethanone O-2,4-dinitrophenyloxime

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Chemical Property of (1-benzyl-4,6-dimethoxyindol-2-yl)-phenylmethanone O-2,4-dinitrophenyloxime

Chemical Property:

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Technology Process of (1-benzyl-4,6-dimethoxyindol-2-yl)-phenylmethanone O-2,4-dinitrophenyloxime

There total 4 articles about (1-benzyl-4,6-dimethoxyindol-2-yl)-phenylmethanone O-2,4-dinitrophenyloxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 945620-14-4
(1-benzyl-4,6-dimethoxyindol-2-yl)-phenylmethanone oxime

: 70-34-8,65727-75-5
2,4-Dinitrofluorobenzene

: 945620-15-5
(1-benzyl-4,6-dimethoxyindol-2-yl)-phenylmethanone O-2,4-dinitrophenyloxime

Guidance literature:: With sodium; In ethanol;
DOI:10.1016/j.tet.2007.04.087

Reference yield:

: 945620-13-3
2-benzoyl-1-benzyl-4,6-dimethoxyindole

: 945620-15-5
(1-benzyl-4,6-dimethoxyindol-2-yl)-phenylmethanone O-2,4-dinitrophenyloxime

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / hydroxylamine hydrochloride; pyridine / ethanol / 19 h / Heating

2: 91 percent / sodium / ethanol

With pyridine; hydroxylamine hydrochloride; sodium; In ethanol;
DOI:10.1016/j.tet.2007.04.087

Reference yield:

: 100-39-0
benzyl bromide

: 945620-15-5
(1-benzyl-4,6-dimethoxyindol-2-yl)-phenylmethanone O-2,4-dinitrophenyloxime

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / potassium hydroxide / dimethylsulfoxide / 2 h / 20 °C

2: 81 percent / hydroxylamine hydrochloride; pyridine / ethanol / 19 h / Heating

3: 91 percent / sodium / ethanol

With pyridine; potassium hydroxide; hydroxylamine hydrochloride; sodium; In ethanol; dimethyl sulfoxide;
DOI:10.1016/j.tet.2007.04.087