(E)-4-[1-Benzylamino-eth-(Z)-ylidene]-pent-2-enedioic acid dimethyl ester

Base Information

Chemical Name:(E)-4-[1-Benzylamino-eth-(Z)-ylidene]-pent-2-enedioic acid dimethyl ester
CAS No.:374559-45-2
Molecular Formula:C₁₆H₁₉NO₄
Molecular Weight:289.331
Hs Code.:

Synonyms:(E)-4-[1-Benzylamino-eth-(Z)-ylidene]-pent-2-enedioic acid dimethyl ester

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Chemical Property of (E)-4-[1-Benzylamino-eth-(Z)-ylidene]-pent-2-enedioic acid dimethyl ester

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Technology Process of (E)-4-[1-Benzylamino-eth-(Z)-ylidene]-pent-2-enedioic acid dimethyl ester

There total 4 articles about (E)-4-[1-Benzylamino-eth-(Z)-ylidene]-pent-2-enedioic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 105-45-3
acetoacetic acid methyl ester

: 922-67-8
propynoic acid methyl ester

: 100-46-9
benzylamine

: 374559-45-2
(E)-4-[1-Benzylamino-eth-(Z)-ylidene]-pent-2-enedioic acid dimethyl ester

Guidance literature:: acetoacetic acid methyl ester; benzylamine; In methanol; for 2h; Heating;

propynoic acid methyl ester; In methanol; for 48h; Heating;
DOI:10.1055/s-2002-19310

Reference yield:

: 105-45-3
acetoacetic acid methyl ester

: 374559-45-2
(E)-4-[1-Benzylamino-eth-(Z)-ylidene]-pent-2-enedioic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / methanol / 12 h / Heating

2: 48 h / Heating

In methanol;
DOI:10.1055/s-2001-16790

Reference yield:

: 100-46-9
benzylamine

: 374559-45-2
(E)-4-[1-Benzylamino-eth-(Z)-ylidene]-pent-2-enedioic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / methanol / 12 h / Heating

2: 48 h / Heating

In methanol;
DOI:10.1055/s-2001-16790