9-<3'-brom-2'-(Methoxymethoxy)phenyl>-1-<(2RS)-2-tetrahydropyranyloxy>nonan

Base Information

Chemical Name:9-<3'-brom-2'-(Methoxymethoxy)phenyl>-1-<(2RS)-2-tetrahydropyranyloxy>nonan
CAS No.:112999-89-0
Molecular Formula:C₂₂H₃₅BrO₄
Molecular Weight:443.421
Hs Code.:

Synonyms:9-<3'-brom-2'-(Methoxymethoxy)phenyl>-1-<(2RS)-2-tetrahydropyranyloxy>nonan

Suppliers and Price of 9-<3'-brom-2'-(Methoxymethoxy)phenyl>-1-<(2RS)-2-tetrahydropyranyloxy>nonan

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-<3'-brom-2'-(Methoxymethoxy)phenyl>-1-<(2RS)-2-tetrahydropyranyloxy>nonan

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Technology Process of 9-<3'-brom-2'-(Methoxymethoxy)phenyl>-1-<(2RS)-2-tetrahydropyranyloxy>nonan

There total 4 articles about 9-<3'-brom-2'-(Methoxymethoxy)phenyl>-1-<(2RS)-2-tetrahydropyranyloxy>nonan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 107495-58-9
9-<2'-(Methoxymethoxy)phenyl>-1-<(RS)-2-tetrahydropyranyloxy>nonan

: 106-93-4
ethylene dibromide

: 112999-89-0
9-<3'-brom-2'-(Methoxymethoxy)phenyl>-1-<(2RS)-2-tetrahydropyranyloxy>nonan

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; for 1h; Heating;

Reference yield:

: 55362-80-6
9-bromononan-1-ol

: 112999-89-0
9-<3'-brom-2'-(Methoxymethoxy)phenyl>-1-<(2RS)-2-tetrahydropyranyloxy>nonan

Guidance literature:: Multi-step reaction with 3 steps

1: pyridinium-p-toluenesulfonate / CH₂Cl₂ / 3 h / 0 - 5 °C

2: 80 percent / 1.5 M BuLi, N,N,N',N'-tetramethylethylenediamine / hexane; tetrahydrofuran

3: 36 percent / 1.4 M BuLi, N,N,N',N'-tetramethylethylenediamine / hexane; tetrahydrofuran / 1 h / Heating

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; pyridinium p-toluenesulfonate; In tetrahydrofuran; hexane; dichloromethane;

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 112999-89-0
9-<3'-brom-2'-(Methoxymethoxy)phenyl>-1-<(2RS)-2-tetrahydropyranyloxy>nonan

Guidance literature:: Multi-step reaction with 3 steps

1: pyridinium-p-toluenesulfonate / CH₂Cl₂ / 3 h / 0 - 5 °C

2: 80 percent / 1.5 M BuLi, N,N,N',N'-tetramethylethylenediamine / hexane; tetrahydrofuran

3: 36 percent / 1.4 M BuLi, N,N,N',N'-tetramethylethylenediamine / hexane; tetrahydrofuran / 1 h / Heating

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; pyridinium p-toluenesulfonate; In tetrahydrofuran; hexane; dichloromethane;