5,11,17,23,29,35-hexabenzyloxy-37,38,39,40,41,42-hexahydroxycalix[6]arene

Base Information

• Chemical Name: 5,11,17,23,29,35-hexabenzyloxy-37,38,39,40,41,42-hexahydroxycalix[6]arene
• CAS No.: 327154-31-4
• Molecular Formula: C₈₄H₇₂O₁₂
• Molecular Weight: 1273.49

Synonyms:5,11,17,23,29,35-hexabenzyloxy-37,38,39,40,41,42-hexahydroxycalix[6]arene

Chemical Property of 5,11,17,23,29,35-hexabenzyloxy-37,38,39,40,41,42-hexahydroxycalix[6]arene

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Technology Process of 5,11,17,23,29,35-hexabenzyloxy-37,38,39,40,41,42-hexahydroxycalix[6]arene

There total 4 articles about 5,11,17,23,29,35-hexabenzyloxy-37,38,39,40,41,42-hexahydroxycalix[6]arene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 4-Benzyloxyphenol (103-16-2) → 5,11,17,23,29,35-hexabenzyloxy-37,38,39,40,41,42-hexahydroxycalix[6]arene (327154-31-4)

Guidance literature:

With cesium hydroxide; In 5,5-dimethyl-1,3-cyclohexadiene; water; for 5.5h; Inert atmosphere; Dean-Stark; Reflux;

Reference yield: 48.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 4-Benzyloxyphenol (103-16-2) → 5,11,17,23,29,35-hexabenzyloxy-37,38,39,40,41,42-hexahydroxycalix[6]arene (327154-31-4) + p-(benzyloxy)calix[7]arene + 5,11,17,23,29,35,41,47-octakis(benzyloxy)-49,50,51,52,53,54,55,56-octahydroxycalix<8>arene (193743-53-2)

Guidance literature:

With sodium hydroxide; In 5,5-dimethyl-1,3-cyclohexadiene; water; for 4.5h; Inert atmosphere; Dean-Stark; Reflux;

Reference yield: 30.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 4-Benzyloxyphenol (103-16-2) → p-(benzyloxy)calix[12]arene + p-(benzyloxy)calix[13]arene + p-(benzyloxy)calix[14]arene + p-(benzyloxy)calix[15]arene + 5,11,17,23,29,35-hexabenzyloxy-37,38,39,40,41,42-hexahydroxycalix[6]arene (327154-31-4) + 5,11,17,23,29,35,41,47-octakis(benzyloxy)-49,50,51,52,53,54,55,56-octahydroxycalix<8>arene (193743-53-2)

Guidance literature:

With rubidium hydroxide; In 5,5-dimethyl-1,3-cyclohexadiene; water; for 6h; Dean-Stark; Reflux;

upstream raw materials:

formaldehyd

4-Benzyloxyphenol

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