2,3,6-triphenyl-4-oxopiperidine semicarbazone

Base Information

• Chemical Name: 2,3,6-triphenyl-4-oxopiperidine semicarbazone
• CAS No.: 124069-19-8
• Molecular Formula: C₂₄H₂₄N₄O
• Molecular Weight: 384.481
• Mol file: 124069-19-8.mol

Synonyms:2,3,6-triphenyl-4-oxopiperidine semicarbazone

Chemical Property of 2,3,6-triphenyl-4-oxopiperidine semicarbazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3,6-triphenyl-4-oxopiperidine semicarbazone

There total 3 articles about 2,3,6-triphenyl-4-oxopiperidine semicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

semicarbazide hydrochloride (563-41-7) + 2,3,6-triphenyl-piperidin-4-one (124069-05-2) → 2,3,6-triphenyl-4-oxopiperidine semicarbazone (124069-19-8)

Guidance literature:

With sodium acetate; In methanol; for 4h; Heating;

DOI:10.1080/10426509708043502

Reference yield:

benzaldehyde (100-52-7) → 2,3,6-triphenyl-4-oxopiperidine semicarbazone (124069-19-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 43 percent / ammonium acetate / acetic acid / 15 h / 20 °C

2: 31 percent / sodium acetate / ethanol / 0.25 h

With ammonium acetate; sodium acetate; In ethanol; acetic acid;

DOI:10.1007/BF00758420

Reference yield:

1-phenyl-acetone (103-79-7,136675-26-8) → 2,3,6-triphenyl-4-oxopiperidine semicarbazone (124069-19-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 43 percent / ammonium acetate / acetic acid / 15 h / 20 °C

2: 31 percent / sodium acetate / ethanol / 0.25 h

With ammonium acetate; sodium acetate; In ethanol; acetic acid;

DOI:10.1007/BF00758420

upstream raw materials:

semicarbazide hydrochloride

2,3,6-triphenyl-piperidin-4-one

benzaldehyde

1-phenyl-acetone