Technology Process of C17H21NO6
There total 8 articles about C17H21NO6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 20 ℃;
DOI:10.1021/jo010838k
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 79 percent / AcOH / ethanol / 3 h / Heating
2: 72 percent / HCl / acetone / 2 h / 0 °C
3: 88 percent / H2 / 10percent Pd/C / ethanol / 20 °C
4: 86 percent / pyridine / CH2Cl2 / 5 h / 0 °C
5: 90 percent / (CH3)3COK / acetonitrile / 0.5 h / 20 °C
6: 70 percent / imidazole / acetonitrile / 24 h / 20 °C
7: 99 percent / NaH / tetrahydrofuran
8: 96 percent / TBAF / tetrahydrofuran / 20 °C
With
pyridine; 1H-imidazole; hydrogenchloride; potassium tert-butylate; tetrabutyl ammonium fluoride; hydrogen; sodium hydride; acetic acid;
10percent Pd/C;
In
tetrahydrofuran; ethanol; dichloromethane; acetone; acetonitrile;
DOI:10.1021/jo010838k
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 72 percent / HCl / acetone / 2 h / 0 °C
2: 88 percent / H2 / 10percent Pd/C / ethanol / 20 °C
3: 86 percent / pyridine / CH2Cl2 / 5 h / 0 °C
4: 90 percent / (CH3)3COK / acetonitrile / 0.5 h / 20 °C
5: 70 percent / imidazole / acetonitrile / 24 h / 20 °C
6: 99 percent / NaH / tetrahydrofuran
7: 96 percent / TBAF / tetrahydrofuran / 20 °C
With
pyridine; 1H-imidazole; hydrogenchloride; potassium tert-butylate; tetrabutyl ammonium fluoride; hydrogen; sodium hydride;
10percent Pd/C;
In
tetrahydrofuran; ethanol; dichloromethane; acetone; acetonitrile;
DOI:10.1021/jo010838k
