<1(1R,3R,4R),1E,3R>-3-hydroxy-5-<(4-methoxybenzyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene

Base Information

• Chemical Name: <1(1R,3R,4R),1E,3R>-3-hydroxy-5-<(4-methoxybenzyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene
• CAS No.: 136457-93-7
• Molecular Formula: C₃₂H₅₆O₅Si
• Molecular Weight: 548.879

Synonyms:<1(1R,3R,4R),1E,3R>-3-hydroxy-5-<(4-methoxybenzyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene

Chemical Property of <1(1R,3R,4R),1E,3R>-3-hydroxy-5-<(4-methoxybenzyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of <1(1R,3R,4R),1E,3R>-3-hydroxy-5-<(4-methoxybenzyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene

There total 2 articles about <1(1R,3R,4R),1E,3R>-3-hydroxy-5-<(4-methoxybenzyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2-dimethyl-3-(4-methoxyphenylmethoxy)propionaldehyde (92156-87-1) + (1R,2R,4R)-4-<(E)-2-bromo-1-propen-1-yl>-2-methoxy-1-<(triisopropylsilyl)oxy>cyclohexane (122948-78-1) → <1(1R,3R,4R),1E,3S>-3-hydroxy-5-<(4-methoxybenzyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene (136358-40-2,136457-93-7) + <1(1R,3R,4R),1E,3R>-3-hydroxy-5-<(4-methoxybenzyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene (136457-93-7)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given;

Reference yield:

2,2-dimethyl-3-(4-methoxyphenylmethoxy)propionaldehyde (92156-87-1) + (1R,2R,4R)-4-<(E)-2-bromo-1-propen-1-yl>-2-methoxy-1-<(triisopropylsilyl)oxy>cyclohexane (122948-78-1) → <1(1R,3R,4R),1E,3S>-3-hydroxy-5-<(4-methoxybenzyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene (136358-40-2,136457-93-7) + <1(1R,3R,4R),1E,3R>-3-hydroxy-5-<(4-methoxybenzyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene (136457-93-7)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given;

Reference yield: 91.6%

(S)-(-)-1-(tert-butoxycarbonyl)-2-piperidinecarboxylic acid (26250-84-0) + <1(1R,3R,4R),1E,3S>-3-hydroxy-5-<(4-methoxybenzyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene (136358-40-2,136457-93-7) → <1(1R,3R,4R),1E,3(2S),3S>-3-<<<-N-(tert-butoxycarbonyl)piperidin-2-yl>carbonyl>oxy>-5-<(4-methoxybenzyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene (136358-57-1)

Guidance literature:

With 4-pyrrolidin-1-ylpyridine; diisopropyl-carbodiimide; In dichloromethane; at -20 ℃; for 1h;

upstream raw materials:

2,2-dimethyl-3-(4-methoxyphenylmethoxy)propionaldehyde

(1R,2R,4R)-4-<(E)-2-bromo-1-propen-1-yl>-2-methoxy-1-<(triisopropylsilyl)oxy>cyclohexane

Downstream raw materials:

<1(1R,3R,4R),1E,3(2S),3S>-3-<<<-N-(tert-butoxycarbonyl)piperidin-2-yl>carbonyl>oxy>-5-<(4-methoxybenzyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene

<1(1R,3R,4R),1E,3(2S),3S>-3-<(piperidin-2-ylcarbonyl)oxy>-5-<(trimethylsilyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene

(E)-(1R,9S,12R,18S,19S,20S,21S,23R)-1-Hydroxy-12-[(E)-2-((1R,3R,4R)-4-hydroxy-3-methoxy-cyclohexyl)-1-methyl-vinyl]-18-isopropyl-19,21-dimethoxy-13,13,23-trimethyl-11,17,24-trioxa-4-aza-tricyclo[18.3.1.0^4,9]tetracos-14-ene-2,3,10,16-tetraone

C₅₃H₉₇NO₁₂Si₂

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 136457-93-7 <1(1R,3R,4R),1E,3R>-3-hydroxy-5-<(4-methoxybenzyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene

Send

Send

Metric Ton KG G Pound L ML

Send

Send