dimethyl 7-allyl-3-tosyl-6,7,10,13-tetrahydro-5H-7,13-diazacyclodeca[a]indene-8,9-dicarboxylate

Base Information

• Chemical Name: dimethyl 7-allyl-3-tosyl-6,7,10,13-tetrahydro-5H-7,13-diazacyclodeca[a]indene-8,9-dicarboxylate
• CAS No.: 1068441-77-9
• Molecular Formula: C₂₉H₃₀N₂O₆S
• Molecular Weight: 534.633

Synonyms:dimethyl 7-allyl-3-tosyl-6,7,10,13-tetrahydro-5H-7,13-diazacyclodeca[a]indene-8,9-dicarboxylate

Chemical Property of dimethyl 7-allyl-3-tosyl-6,7,10,13-tetrahydro-5H-7,13-diazacyclodeca[a]indene-8,9-dicarboxylate

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Technology Process of dimethyl 7-allyl-3-tosyl-6,7,10,13-tetrahydro-5H-7,13-diazacyclodeca[a]indene-8,9-dicarboxylate

There total 4 articles about dimethyl 7-allyl-3-tosyl-6,7,10,13-tetrahydro-5H-7,13-diazacyclodeca[a]indene-8,9-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

2-allyl-9-tosyl-1-vinyl-2,3,4,9-tetrahydro-1H-β-carboline (1068441-76-8) + dimethyl acetylenedicarboxylate (762-42-5) → dimethyl 7-allyl-3-tosyl-6,7,10,13-tetrahydro-5H-7,13-diazacyclodeca[a]indene-8,9-dicarboxylate (1068441-77-9) + dimethyl 2-(allyl(2-(2-((E)-6-methoxy-4-(methoxycarbonyl)-5,6-dioxohex-1-enyl)-1-tosyl-1H-indol-3-yl)ethyl)amino)maleate (1397693-93-4)

Guidance literature:

In dichloromethane; at 20 ℃; for 48h; Inert atmosphere;

DOI:10.1039/c2ob25755f

Reference yield: 55.0%

2-allyl-9-tosyl-1-vinyl-2,3,4,9-tetrahydro-1H-β-carboline (1068441-76-8) + dimethyl acetylenedicarboxylate (762-42-5) → dimethyl 7-allyl-3-tosyl-6,7,10,13-tetrahydro-5H-7,13-diazacyclodeca[a]indene-8,9-dicarboxylate (1068441-77-9) + dimethyl (E)-2-(9-tosyl-1-vinyl-1,3,4,9-tetrahydro-2H-β-carbolin-2-yl)but-2-enedioate (1397693-94-5) + dimethyl 2-(allyl(2-(2-((E)-6-methoxy-4-(methoxycarbonyl)-5,6-dioxohex-1-enyl)-1-tosyl-1H-indol-3-yl)ethyl)amino)maleate (1397693-93-4)

Guidance literature:

With gold(III) chloride; In dichloromethane; at 0 - 20 ℃; for 3h; Inert atmosphere;

DOI:10.1039/c2ob25755f

Reference yield: 41.0%

2-allyl-9-tosyl-1-vinyl-2,3,4,9-tetrahydro-1H-β-carboline (1068441-76-8) + dimethyl acetylenedicarboxylate (762-42-5) → dimethyl 7-allyl-3-tosyl-6,7,10,13-tetrahydro-5H-7,13-diazacyclodeca[a]indene-8,9-dicarboxylate (1068441-77-9)

Guidance literature:

In dichloromethane; for 2.5h; Inert atmosphere; Heating;

DOI:10.1039/c2ob25755f

upstream raw materials:

2-allyl-9-tosyl-1-vinyl-2,3,4,9-tetrahydro-1H-β-carboline

dimethyl acetylenedicarboxylate

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