C₂₁H₂₉NO₇

Base Information

Chemical Name:C₂₁H₂₉NO₇
CAS No.:951024-81-0
Molecular Formula:C₂₁H₂₉NO₇
Molecular Weight:407.464
Hs Code.:

C<sub>21</sub>H<sub>29</sub>NO<sub>7</sub>

Synonyms:C₂₁H₂₉NO₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₂₉NO₇

Chemical Property:

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Technology Process of C₂₁H₂₉NO₇

There total 10 articles about C₂₁H₂₉NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 951024-76-3
C₁₆H₂₁NO₆

: 3282-30-2
pivaloyl chloride

: 951024-81-0
C₂₁H₂₉NO₇

Guidance literature:: With pyridine; at 23 ℃;
DOI:10.1021/ol701446y

Reference yield:

: 951024-71-8
C₂₆H₂₉O₅N

: 951024-81-0
C₂₁H₂₉NO₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: aq. H₂O₂; LiOH*H₂O / tetrahydrofuran / 0 - 23 °C

1.2: 91 percent / tetrabutylammonium iodide; K₂CO₃ / dimethylformamide / 2 h / 23 °C

2.1: ozone / methanol / -78 °C

2.2: 87 percent / dimethyl sulfide / methanol / -78 °C

3.1: 224 mg / H₂ / Pd/C / methanol / 23 °C

4.1: 78 percent / 2,2,2-trifluoro-ethanol / 23 °C

5.1: 87 percent / dl-camphorsulfonic acid / methanol / 3 h / 60 °C

6.1: 88 percent / pyridine / 1 h / 23 °C

7.1: 94 percent / dl-camphorsulfonic acid / benzene / 2 h / 70 °C

8.1: 87 percent / triethylamine / 23 °C

9.1: 65 percent / pyridine / 23 °C

With pyridine; lithium hydroxide; camphor-10-sulfonic acid; hydrogen; dihydrogen peroxide; ozone; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; 2,2,2-trifluoroethanol; benzene;
DOI:10.1021/ol701446y

Reference yield:

: C₂₃H₂₅O₅N

: 951024-81-0
C₂₁H₂₉NO₇

Guidance literature:: Multi-step reaction with 10 steps

1.1: 82 percent / p-toluenesulfonic acid monohydrate / 23 °C

2.1: aq. H₂O₂; LiOH*H₂O / tetrahydrofuran / 0 - 23 °C

2.2: 91 percent / tetrabutylammonium iodide; K₂CO₃ / dimethylformamide / 2 h / 23 °C

3.1: ozone / methanol / -78 °C

3.2: 87 percent / dimethyl sulfide / methanol / -78 °C

4.1: 224 mg / H₂ / Pd/C / methanol / 23 °C

5.1: 78 percent / 2,2,2-trifluoro-ethanol / 23 °C

6.1: 87 percent / dl-camphorsulfonic acid / methanol / 3 h / 60 °C

7.1: 88 percent / pyridine / 1 h / 23 °C

8.1: 94 percent / dl-camphorsulfonic acid / benzene / 2 h / 70 °C

9.1: 87 percent / triethylamine / 23 °C

10.1: 65 percent / pyridine / 23 °C

With pyridine; lithium hydroxide; camphor-10-sulfonic acid; hydrogen; dihydrogen peroxide; toluene-4-sulfonic acid; ozone; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; 2,2,2-trifluoroethanol; benzene;
DOI:10.1021/ol701446y