(E)-N-(but-2-en-1-yl)-N-(1-(4-methoxyphenyl)-5-phenylpyrazolo[5,1-a]isoquinolin-2-yl)-4-methylbenzenesulfonamide

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Chemical Name:(E)-N-(but-2-en-1-yl)-N-(1-(4-methoxyphenyl)-5-phenylpyrazolo[5,1-a]isoquinolin-2-yl)-4-methylbenzenesulfonamide
CAS No.:1379536-73-8
Molecular Formula:C₃₅H₃₁N₃O₃S
Molecular Weight:573.715
Hs Code.:

Synonyms:(E)-N-(but-2-en-1-yl)-N-(1-(4-methoxyphenyl)-5-phenylpyrazolo[5,1-a]isoquinolin-2-yl)-4-methylbenzenesulfonamide

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Chemical Property of (E)-N-(but-2-en-1-yl)-N-(1-(4-methoxyphenyl)-5-phenylpyrazolo[5,1-a]isoquinolin-2-yl)-4-methylbenzenesulfonamide

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Technology Process of (E)-N-(but-2-en-1-yl)-N-(1-(4-methoxyphenyl)-5-phenylpyrazolo[5,1-a]isoquinolin-2-yl)-4-methylbenzenesulfonamide

There total 1 articles about (E)-N-(but-2-en-1-yl)-N-(1-(4-methoxyphenyl)-5-phenylpyrazolo[5,1-a]isoquinolin-2-yl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 928154-75-0
N-allyl-N-((4-methoxyphenyl)ethynyl)-4-methylbenzenesulfonamide

: 75586-32-2
2-phenylethynylbenzaldehyde p-toluenesulphonylhydrazone

: 1379536-69-2
N-(but-2-en-1-yl)-N-(1-(4-methoxyphenyl)-5-phenylpyrazolo[5,1-a]isoquinolin-2-yl)-4-methylbenzenesulfonamide

: 1379536-73-8
(E)-N-(but-2-en-1-yl)-N-(1-(4-methoxyphenyl)-5-phenylpyrazolo[5,1-a]isoquinolin-2-yl)-4-methylbenzenesulfonamide

Guidance literature:: 2-phenylethynylbenzaldehyde p-toluenesulphonylhydrazone; With silver trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 70 ℃; for 3h; Inert atmosphere;

N-allyl-N-((4-methoxyphenyl)ethynyl)-4-methylbenzenesulfonamide; With palladium diacetate; caesium carbonate; triphenylphosphine; In 1,2-dichloro-ethane; toluene; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol301023m