3-<<6-<(chloroacetyl)amino>-1-oxohexyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

Base Information

Chemical Name:3-<<6-<(chloroacetyl)amino>-1-oxohexyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid
CAS No.:160982-41-2
Molecular Formula:C₁₉H₂₄ClI₃N₂O₄
Molecular Weight:760.577
Hs Code.:

Synonyms:3-<<6-<(chloroacetyl)amino>-1-oxohexyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-<<6-<(chloroacetyl)amino>-1-oxohexyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

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Technology Process of 3-<<6-<(chloroacetyl)amino>-1-oxohexyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

There total 2 articles about 3-<<6-<(chloroacetyl)amino>-1-oxohexyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 79-37-8
oxalyl dichloride

: 61435-75-4
6-<(chloroacetyl)amino>hexanoic acid

: 96-83-3
iopanoic acid

: 160982-41-2
3-<<6-<(chloroacetyl)amino>-1-oxohexyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

Guidance literature:: With pyridine; hydrogenchloride; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 61435-75-4
6-<(chloroacetyl)amino>hexanoic acid

: 96-83-3
iopanoic acid

: 160982-41-2
3-<<6-<(chloroacetyl)amino>-1-oxohexyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

Guidance literature:: With pyridine; oxalyl dichloride; Yield given. Multistep reaction; 1.) DMF, CH₂Cl₂, 5 deg C, 1 h, 2.) THF, CH₃CN, 5 deg C, then 40 deg C, 2 h, 3.) THF, reflux, 3 h;