4-methoxyphenyl (3,4-di-O-acetyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:4-methoxyphenyl (3,4-di-O-acetyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside
CAS No.:774591-93-4
Molecular Formula:C₅₄H₅₈Cl₃NO₁₅
Molecular Weight:1067.41
Hs Code.:

4-methoxyphenyl (3,4-di-O-acetyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Synonyms:4-methoxyphenyl (3,4-di-O-acetyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Chemical Property of 4-methoxyphenyl (3,4-di-O-acetyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Technology Process of 4-methoxyphenyl (3,4-di-O-acetyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

There total 4 articles about 4-methoxyphenyl (3,4-di-O-acetyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 774591-92-3
4-methoxyphenyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 219518-11-3
ethyl 3,4-di-O-acetyl-6-O-benzyl-2-deoxy-2-<<(2,2,2-trichloroethoxy)carbonyl>amino>-1-thio-β-D-galactopyranoside

: 774591-93-4
4-methoxyphenyl (3,4-di-O-acetyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: With 3 A molecular sieve; silver trifluoromethanesulfonate; Iodine monochloride; In dichloromethane; at -45 ℃; for 1h;
DOI:10.1021/jo049184g

Reference yield:

: 765952-64-5
4-methoxyphenyl 2,3-di-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

: 774591-93-4
4-methoxyphenyl (3,4-di-O-acetyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / NaBH₃CN; molecular sieves 3 Angstroem; HCl / tetrahydrofuran; diethyl ether / 2 h / 0 °C / pH 2

2: AgOTf; ICl

With hydrogenchloride; 3 A molecular sieve; silver trifluoromethanesulfonate; Iodine monochloride; sodium cyanoborohydride; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo049184g

Reference yield:

: 100-39-0
benzyl bromide

: 774591-93-4
4-methoxyphenyl (3,4-di-O-acetyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / NaH / dimethylformamide / 18 h

2: 88 percent / NaBH₃CN; molecular sieves 3 Angstroem; HCl / tetrahydrofuran; diethyl ether / 2 h / 0 °C / pH 2

3: AgOTf; ICl

With hydrogenchloride; 3 A molecular sieve; silver trifluoromethanesulfonate; Iodine monochloride; sodium hydride; sodium cyanoborohydride; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/jo049184g