benzyl (6-(2-(4-((tert-butyldimethylsilyl)oxy)-3-methoxyphenyl)acetamido)hexyl)carbamate

Base Information

Chemical Name:benzyl (6-(2-(4-((tert-butyldimethylsilyl)oxy)-3-methoxyphenyl)acetamido)hexyl)carbamate
CAS No.:1394822-19-5
Molecular Formula:C₂₉H₄₄N₂O₅Si
Molecular Weight:528.764
Hs Code.:

Synonyms:benzyl (6-(2-(4-((tert-butyldimethylsilyl)oxy)-3-methoxyphenyl)acetamido)hexyl)carbamate

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Chemical Property of benzyl (6-(2-(4-((tert-butyldimethylsilyl)oxy)-3-methoxyphenyl)acetamido)hexyl)carbamate

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Technology Process of benzyl (6-(2-(4-((tert-butyldimethylsilyl)oxy)-3-methoxyphenyl)acetamido)hexyl)carbamate

There total 5 articles about benzyl (6-(2-(4-((tert-butyldimethylsilyl)oxy)-3-methoxyphenyl)acetamido)hexyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1394822-10-6
2,5-dioxopyrrolidin-1-yl 2-(4-(tert-butyldimethylsilyloxy)-3-methoxyphenyl)acetate

: 66095-18-9
N-benzyloxycarbonyl-1,6-hexanediamine

: 1394822-19-5
benzyl (6-(2-(4-((tert-butyldimethylsilyl)oxy)-3-methoxyphenyl)acetamido)hexyl)carbamate

Guidance literature:: N-benzyloxycarbonyl-1,6-hexanediamine; With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h;

2,5-dioxopyrrolidin-1-yl 2-(4-(tert-butyldimethylsilyloxy)-3-methoxyphenyl)acetate; In N,N-dimethyl-formamide; at 20 ℃; for 14h; Inert atmosphere;
DOI:10.1002/anie.201201451

Reference yield: 83.0%

: 1394822-10-6
2,5-dioxopyrrolidin-1-yl 2-(4-(tert-butyldimethylsilyloxy)-3-methoxyphenyl)acetate

: hexamethylenediamine hydrochloride

: 1394822-19-5
benzyl (6-(2-(4-((tert-butyldimethylsilyl)oxy)-3-methoxyphenyl)acetamido)hexyl)carbamate

Guidance literature:: hexamethylenediamine hydrochloride; With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h;

2,5-dioxopyrrolidin-1-yl 2-(4-(tert-butyldimethylsilyloxy)-3-methoxyphenyl)acetate; In N,N-dimethyl-formamide; at 20 ℃; for 14h; Inert atmosphere;
DOI:10.1002/anie.201305645

Reference yield:

: 1344662-01-6
2-(4-((tert-butyldimethylsilyl)oxy)-3-methoxyphenyl)acetic acid

: 1394822-19-5
benzyl (6-(2-(4-((tert-butyldimethylsilyl)oxy)-3-methoxyphenyl)acetamido)hexyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dicyclohexyl-carbodiimide / tetrahydrofuran / 14 h / 0 - 25 °C / Inert atmosphere

2.1: triethylamine / N,N-dimethyl-formamide / 0.08 h / 20 °C

2.2: 14 h / 20 °C / Inert atmosphere

With triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/anie.201201451