(S)-2-((Z)-2-{(S)-2-[(R)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-methyl-butyrylamino]-3-tritylsulfanyl-propionylamino}-but-2-enoylamino)-3-methyl-butyric acid

Base Information

Chemical Name:(S)-2-((Z)-2-{(S)-2-[(R)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-methyl-butyrylamino]-3-tritylsulfanyl-propionylamino}-but-2-enoylamino)-3-methyl-butyric acid
CAS No.:1089192-64-2
Molecular Formula:C₅₁H₅₄N₄O₇S
Molecular Weight:867.078
Hs Code.:

(S)-2-((Z)-2-{(S)-2-[(R)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-methyl-butyrylamino]-3-tritylsulfanyl-propionylamino}-but-2-enoylamino)-3-methyl-butyric acid

Synonyms:(S)-2-((Z)-2-{(S)-2-[(R)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-methyl-butyrylamino]-3-tritylsulfanyl-propionylamino}-but-2-enoylamino)-3-methyl-butyric acid

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Chemical Property of (S)-2-((Z)-2-{(S)-2-[(R)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-methyl-butyrylamino]-3-tritylsulfanyl-propionylamino}-but-2-enoylamino)-3-methyl-butyric acid

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Technology Process of (S)-2-((Z)-2-{(S)-2-[(R)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-methyl-butyrylamino]-3-tritylsulfanyl-propionylamino}-but-2-enoylamino)-3-methyl-butyric acid

There total 1 articles about (S)-2-((Z)-2-{(S)-2-[(R)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-methyl-butyrylamino]-3-tritylsulfanyl-propionylamino}-but-2-enoylamino)-3-methyl-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₆H₄₄N₄O₅S

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 1089192-64-2
(S)-2-((Z)-2-{(S)-2-[(R)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-methyl-butyrylamino]-3-tritylsulfanyl-propionylamino}-but-2-enoylamino)-3-methyl-butyric acid

Guidance literature:: C₃₆H₄₄N₄O₅S; (fluorenylmethoxy)carbonyl chloride; With sodium hydrogencarbonate; sodium carbonate; In tetrahydrofuran; water; Cooling with ice; Saturated solution;

With hydrogenchloride; In tetrahydrofuran; water; pH=4 - 5;
DOI:10.1021/jo801866z

Reference yield: 34.0%

: 1043577-31-6
(S,E)-2-(trimethylsilyl)ethyl 3-(((S)-2-amino-3-methylbutanoyl)oxy)-7-(tritylthio)hept-4-enoate

: 1089192-64-2
(S)-2-((Z)-2-{(S)-2-[(R)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-methyl-butyrylamino]-3-tritylsulfanyl-propionylamino}-but-2-enoylamino)-3-methyl-butyric acid

: 1089192-65-3
C₈₂H₉₀N₄O₉S₂Si

Guidance literature:: With 1-methyl-1H-imidazole; 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; In dichloromethane; at 20 ℃; for 6.66667h; Cooling with ice;
DOI:10.1021/jo801866z