N-benzyloxycarbonyl-O-t-butyl-L-tyrosyl-α-aminoisobutyrylglycine ethyl ester

Base Information

Chemical Name:N-benzyloxycarbonyl-O-t-butyl-L-tyrosyl-α-aminoisobutyrylglycine ethyl ester
CAS No.:98607-22-8
Molecular Formula:C₂₉H₃₉N₃O₇
Molecular Weight:541.645
Hs Code.:

Synonyms:N-benzyloxycarbonyl-O-t-butyl-L-tyrosyl-α-aminoisobutyrylglycine ethyl ester

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Chemical Property of N-benzyloxycarbonyl-O-t-butyl-L-tyrosyl-α-aminoisobutyrylglycine ethyl ester

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Technology Process of N-benzyloxycarbonyl-O-t-butyl-L-tyrosyl-α-aminoisobutyrylglycine ethyl ester

There total 3 articles about N-benzyloxycarbonyl-O-t-butyl-L-tyrosyl-α-aminoisobutyrylglycine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 623-33-6
glycine ethyl ester hydrochloride

: 98607-21-7
N-benzyloxycarbonyl-O-t-butyl-L-tyrosyl-α-aminoisobutyric acid

: 98607-22-8
N-benzyloxycarbonyl-O-t-butyl-L-tyrosyl-α-aminoisobutyrylglycine ethyl ester

Guidance literature:: With 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; In dichloromethane; at 0 - 20 ℃; for 16h;

Reference yield:

: 5545-54-0
N-(benzyloxycarbonyl)-O-(1,1-dimethylethyl)-L-tyrosine

: 98607-22-8
N-benzyloxycarbonyl-O-t-butyl-L-tyrosyl-α-aminoisobutyrylglycine ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 2-chloro-4,6-dimethoxy-1,3,5-triazine (CDMT), N-methylmorpholine, 2.) N-methylmorpholine / 1.) CH₂Cl₂, 0 deg C, 1 h, 2.) CH₂Cl₂, RT, 12 h

2: 86 percent / aq. NaOH / propan-2-ol / 12 h / Ambient temperature

3: 82 percent / 2-chloro-4,6-dimethoxy-1,3,5-triazine (CDMT), N-methylmorpholine (NMM) / CH₂Cl₂ / 16 h / 0 - 20 °C

With 4-methyl-morpholine; sodium hydroxide; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; In dichloromethane; isopropyl alcohol;

Reference yield:

: 98607-20-6
N-benzyloxycarbonyl-O-t-butyl-L-tyrosyl-α-aminoisobutyric acid methyl ester

: 98607-22-8
N-benzyloxycarbonyl-O-t-butyl-L-tyrosyl-α-aminoisobutyrylglycine ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / aq. NaOH / propan-2-ol / 12 h / Ambient temperature

2: 82 percent / 2-chloro-4,6-dimethoxy-1,3,5-triazine (CDMT), N-methylmorpholine (NMM) / CH₂Cl₂ / 16 h / 0 - 20 °C

With 4-methyl-morpholine; sodium hydroxide; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; In dichloromethane; isopropyl alcohol;