Carbonic acid 4-[bis-(2-chloro-ethyl)-amino]-2-methyl-phenyl ester 4-nitro-phenyl ester

Base Information

Chemical Name:Carbonic acid 4-[bis-(2-chloro-ethyl)-amino]-2-methyl-phenyl ester 4-nitro-phenyl ester
CAS No.:156079-38-8
Molecular Formula:C₁₈H₁₈Cl₂N₂O₅
Molecular Weight:413.257
Hs Code.:

Synonyms:Carbonic acid 4-[bis-(2-chloro-ethyl)-amino]-2-methyl-phenyl ester 4-nitro-phenyl ester

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Chemical Property of Carbonic acid 4-[bis-(2-chloro-ethyl)-amino]-2-methyl-phenyl ester 4-nitro-phenyl ester

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Technology Process of Carbonic acid 4-[bis-(2-chloro-ethyl)-amino]-2-methyl-phenyl ester 4-nitro-phenyl ester

There total 5 articles about Carbonic acid 4-[bis-(2-chloro-ethyl)-amino]-2-methyl-phenyl ester 4-nitro-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 7693-46-1
4-Nitrophenyl chloroformate

: 4-[Bis-(2-chloro-ethyl)-amino]-2-methyl-phenol; hydrochloride

: 156079-38-8
Carbonic acid 4-[bis-(2-chloro-ethyl)-amino]-2-methyl-phenyl ester 4-nitro-phenyl ester

Guidance literature:: With triethylamine; In chloroform; for 12h; Ambient temperature;
DOI:10.1021/jm00026a013

Reference yield:

: 2835-96-3
4-amino-2-methylphenol

: 156079-38-8
Carbonic acid 4-[bis-(2-chloro-ethyl)-amino]-2-methyl-phenyl ester 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 30 percent / aq. AcOH / 48 h / Ambient temperature

2: 87 percent / KOH / ethanol / 2 h / Heating

3: 34 percent / CH₃SO₂Cl, pyridine / 0.25 h / 70 °C

4: 98 percent / H₂, HCl / 30percent Pd/C / ethanol; diethyl ether

5: 62 percent / Et₃N / CHCl₃ / 12 h / Ambient temperature

With pyridine; hydrogenchloride; potassium hydroxide; hydrogen; acetic acid; methanesulfonyl chloride; triethylamine; palladium on activated charcoal; In diethyl ether; ethanol; chloroform;
DOI:10.1021/jm00026a013

Reference yield:

: 156079-11-7
4-[Bis-(2-hydroxy-ethyl)-amino]-2-methyl-phenol

: 156079-38-8
Carbonic acid 4-[bis-(2-chloro-ethyl)-amino]-2-methyl-phenyl ester 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / KOH / ethanol / 2 h / Heating

2: 34 percent / CH₃SO₂Cl, pyridine / 0.25 h / 70 °C

3: 98 percent / H₂, HCl / 30percent Pd/C / ethanol; diethyl ether

4: 62 percent / Et₃N / CHCl₃ / 12 h / Ambient temperature

With pyridine; hydrogenchloride; potassium hydroxide; hydrogen; methanesulfonyl chloride; triethylamine; palladium on activated charcoal; In diethyl ether; ethanol; chloroform;
DOI:10.1021/jm00026a013