C₂₈H₃₃N₃O₅

Base Information

Chemical Name:C₂₈H₃₃N₃O₅
CAS No.:1192129-09-1
Molecular Formula:C₂₈H₃₃N₃O₅
Molecular Weight:491.587
Hs Code.:

C<sub>28</sub>H<sub>33</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:C₂₈H₃₃N₃O₅

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Chemical Property of C₂₈H₃₃N₃O₅

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Technology Process of C₂₈H₃₃N₃O₅

There total 8 articles about C₂₈H₃₃N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 6723-30-4
O-2-tetrahydro-2H-pyranhydroxylamine

: 1192129-08-0
C₂₃H₂₄N₂O₄*ClH

: 1192129-09-1
C₂₈H₃₃N₃O₅

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.ejmech.2013.03.061

Reference yield:

: 79099-07-3
N-tert-butyloxycarbonylpiperidin-4-one

: 1192129-09-1
C₂₈H₃₃N₃O₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyrrolidine / 2 h / 72 °C / Microwave irradiation

2.1: triethylamine; palladium diacetate; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 9 h / 100 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.17 h / Inert atmosphere

3.2: 3 h / 80 °C / Inert atmosphere

4.1: hydrogenchloride / 1,4-dioxane / 4 h / 20 °C

5.1: potassium carbonate; sodium tris(acetoxy)borohydride / dichloromethane; water / 3 h / 20 °C

6.1: hydrogenchloride / water; acetic acid / 4 h / 85 °C

7.1: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 20 °C

With pyrrolidine; hydrogenchloride; palladium diacetate; sodium tris(acetoxy)borohydride; sodium hydride; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; tris-(o-tolyl)phosphine; In 1,4-dioxane; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; mineral oil; 2.1: |Heck Reaction;
DOI:10.1016/j.ejmech.2013.03.061

Reference yield:

: 1192127-65-3
C₂₈H₃₂N₂O₆

: 1192129-09-1
C₂₈H₃₃N₃O₅

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / 1,4-dioxane / 4 h / 20 °C

2: potassium carbonate; sodium tris(acetoxy)borohydride / dichloromethane; water / 3 h / 20 °C

3: hydrogenchloride / water; acetic acid / 4 h / 85 °C

4: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 20 °C

With hydrogenchloride; sodium tris(acetoxy)borohydride; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In 1,4-dioxane; dichloromethane; water; acetic acid;
DOI:10.1016/j.ejmech.2013.03.061