C₂₄H₃₄OSSi

Base Information

Chemical Name:C₂₄H₃₄OSSi
CAS No.:1547458-72-9
Molecular Formula:C₂₄H₃₄OSSi
Molecular Weight:398.685
Hs Code.:

Synonyms:C₂₄H₃₄OSSi

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Chemical Property of C₂₄H₃₄OSSi

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Technology Process of C₂₄H₃₄OSSi

There total 3 articles about C₂₄H₃₄OSSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1547458-57-0
C₁₇H₂₈OSSi

: 100-39-0
benzyl bromide

: 1547458-72-9
C₂₄H₃₄OSSi

Guidance literature:: C₁₇H₂₈OSSi; With N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane; In tetrahydrofuran; at -78 - 0 ℃; for 2.5h; Inert atmosphere;

benzyl bromide; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol403709g

Reference yield:

: 70-11-1
α-bromoacetophenone

: 1547458-72-9
C₂₄H₃₄OSSi

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

1.2: 3 h / 0 °C / Inert atmosphere

2.1: potassium hexamethylsilazane; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / 2.5 h / -78 - 0 °C / Inert atmosphere

2.2: 2 h / 0 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane; triethylamine; In tetrahydrofuran;
DOI:10.1021/ol403709g

Reference yield:

: 156275-96-6
triisopropylsilanethiol

: 1547458-72-9
C₂₄H₃₄OSSi

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

1.2: 3 h / 0 °C / Inert atmosphere

2.1: potassium hexamethylsilazane; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / 2.5 h / -78 - 0 °C / Inert atmosphere

2.2: 2 h / 0 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane; triethylamine; In tetrahydrofuran;
DOI:10.1021/ol403709g