Methanesulfonic acid 3-{acetyl-[3-(4-tetradecyloxy-phenyl)-propyl]-amino}-benzyl ester

Base Information

Chemical Name:Methanesulfonic acid 3-{acetyl-[3-(4-tetradecyloxy-phenyl)-propyl]-amino}-benzyl ester
CAS No.:1026886-83-8
Molecular Formula:C₃₃H₅₁NO₅S
Molecular Weight:573.838
Hs Code.:

Synonyms:Methanesulfonic acid 3-{acetyl-[3-(4-tetradecyloxy-phenyl)-propyl]-amino}-benzyl ester

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Chemical Property of Methanesulfonic acid 3-{acetyl-[3-(4-tetradecyloxy-phenyl)-propyl]-amino}-benzyl ester

Chemical Property:

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Technology Process of Methanesulfonic acid 3-{acetyl-[3-(4-tetradecyloxy-phenyl)-propyl]-amino}-benzyl ester

There total 9 articles about Methanesulfonic acid 3-{acetyl-[3-(4-tetradecyloxy-phenyl)-propyl]-amino}-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5597-50-2
3-(4-hydroxyphenyl)propionic acid methyl ester

: 1026886-83-8
Methanesulfonic acid 3-{acetyl-[3-(4-tetradecyloxy-phenyl)-propyl]-amino}-benzyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: potassium carbonate / acetone / Heating

2: aq. KOH / methanol

3: oxalyl chloride, DMF / CH₂Cl₂

4: pyridine / tetrahydrofuran / Ambient temperature

5: LiAlH₄ / tetrahydrofuran

6: pyridine / CH₂Cl₂

7: aq. NaOH / ethanol

8: triethylamine / tetrahydrofuran

With pyridine; potassium hydroxide; sodium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; potassium carbonate; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetone;
DOI:10.1021/jm00104a002

Reference yield:

: 112-71-0
1-Bromotetradecane

: 1026886-83-8
Methanesulfonic acid 3-{acetyl-[3-(4-tetradecyloxy-phenyl)-propyl]-amino}-benzyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: potassium carbonate / acetone / Heating

2: aq. KOH / methanol

3: oxalyl chloride, DMF / CH₂Cl₂

4: pyridine / tetrahydrofuran / Ambient temperature

5: LiAlH₄ / tetrahydrofuran

6: pyridine / CH₂Cl₂

7: aq. NaOH / ethanol

8: triethylamine / tetrahydrofuran

With pyridine; potassium hydroxide; sodium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; potassium carbonate; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetone;
DOI:10.1021/jm00104a002

Reference yield:

: 62442-94-8
3-(4-Tetradecyloxy-phenyl)-propionic acid methyl ester

: 1026886-83-8
Methanesulfonic acid 3-{acetyl-[3-(4-tetradecyloxy-phenyl)-propyl]-amino}-benzyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: aq. KOH / methanol

2: oxalyl chloride, DMF / CH₂Cl₂

3: pyridine / tetrahydrofuran / Ambient temperature

4: LiAlH₄ / tetrahydrofuran

5: pyridine / CH₂Cl₂

6: aq. NaOH / ethanol

7: triethylamine / tetrahydrofuran

With pyridine; potassium hydroxide; sodium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; ethanol; dichloromethane;
DOI:10.1021/jm00104a002