N-(3-Hydroxymethyl-phenyl)-N-[3-(4-tetradecyloxy-phenyl)-propyl]-acetamide

Base Information

Chemical Name:N-(3-Hydroxymethyl-phenyl)-N-[3-(4-tetradecyloxy-phenyl)-propyl]-acetamide
CAS No.:144767-01-1
Molecular Formula:C₃₂H₄₉NO₃
Molecular Weight:495.746
Hs Code.:

Synonyms:N-(3-Hydroxymethyl-phenyl)-N-[3-(4-tetradecyloxy-phenyl)-propyl]-acetamide

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Chemical Property of N-(3-Hydroxymethyl-phenyl)-N-[3-(4-tetradecyloxy-phenyl)-propyl]-acetamide

Chemical Property:

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Technology Process of N-(3-Hydroxymethyl-phenyl)-N-[3-(4-tetradecyloxy-phenyl)-propyl]-acetamide

There total 8 articles about N-(3-Hydroxymethyl-phenyl)-N-[3-(4-tetradecyloxy-phenyl)-propyl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5597-50-2
3-(4-hydroxyphenyl)propionic acid methyl ester

: 144767-01-1
N-(3-Hydroxymethyl-phenyl)-N-[3-(4-tetradecyloxy-phenyl)-propyl]-acetamide

Guidance literature:: Multi-step reaction with 7 steps

1: potassium carbonate / acetone / Heating

2: aq. KOH / methanol

3: oxalyl chloride, DMF / CH₂Cl₂

4: pyridine / tetrahydrofuran / Ambient temperature

5: LiAlH₄ / tetrahydrofuran

6: pyridine / CH₂Cl₂

7: aq. NaOH / ethanol

With pyridine; potassium hydroxide; sodium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; potassium carbonate; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetone;
DOI:10.1021/jm00104a002

Reference yield:

: 1027200-39-0
Acetic acid 3-{acetyl-[3-(4-tetradecyloxy-phenyl)-propyl]-amino}-benzyl ester

: 144767-01-1
N-(3-Hydroxymethyl-phenyl)-N-[3-(4-tetradecyloxy-phenyl)-propyl]-acetamide

Guidance literature:: With sodium hydroxide; In ethanol;
DOI:10.1021/jm00104a002

Reference yield:

: 112-71-0
1-Bromotetradecane

: 144767-01-1
N-(3-Hydroxymethyl-phenyl)-N-[3-(4-tetradecyloxy-phenyl)-propyl]-acetamide

Guidance literature:: Multi-step reaction with 7 steps

1: potassium carbonate / acetone / Heating

2: aq. KOH / methanol

3: oxalyl chloride, DMF / CH₂Cl₂

4: pyridine / tetrahydrofuran / Ambient temperature

5: LiAlH₄ / tetrahydrofuran

6: pyridine / CH₂Cl₂

7: aq. NaOH / ethanol

With pyridine; potassium hydroxide; sodium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; potassium carbonate; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetone;
DOI:10.1021/jm00104a002