3-chloro-4-dimethoxymethyl-2-trifluoromethanesulfonyloxybenzoic acid methyl ester

Base Information

Chemical Name:3-chloro-4-dimethoxymethyl-2-trifluoromethanesulfonyloxybenzoic acid methyl ester
CAS No.:1207343-87-0
Molecular Formula:C₁₂H₁₂ClF₃O₇S
Molecular Weight:392.737
Hs Code.:

Synonyms:3-chloro-4-dimethoxymethyl-2-trifluoromethanesulfonyloxybenzoic acid methyl ester

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Chemical Property of 3-chloro-4-dimethoxymethyl-2-trifluoromethanesulfonyloxybenzoic acid methyl ester

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Technology Process of 3-chloro-4-dimethoxymethyl-2-trifluoromethanesulfonyloxybenzoic acid methyl ester

There total 5 articles about 3-chloro-4-dimethoxymethyl-2-trifluoromethanesulfonyloxybenzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.8%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1207343-86-9
3-chloro-4-dimethoxymethyl-2-hydroxybenzoic acid methyl ester

: 1207343-87-0
3-chloro-4-dimethoxymethyl-2-trifluoromethanesulfonyloxybenzoic acid methyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; Cooling with ice;

Reference yield:

: 56962-10-8
2-chloro-3-hydroxybenzaldehyde

: 1207343-87-0
3-chloro-4-dimethoxymethyl-2-trifluoromethanesulfonyloxybenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride / methanol

2: bromine / chloroform / 20 °C / Cooling with ice

3: hydrogenchloride / methanol / Reflux

4: sodium acetate / palladium diacetate; (diphenylphosphin)ferrocene / 4 h / 90 - 100 °C / 6375.64 Torr / Autoclave

5: triethylamine / dichloromethane / 20 °C / Cooling with ice

With bromine; sodium acetate; triethylamine; hydrogenchloride; (diphenylphosphin)ferrocene; palladium diacetate; In methanol; dichloromethane; chloroform;

Reference yield:

: 860243-44-3
4-bromo-2-chloro-3-hydroxy-benzaldehyde

: 1207343-87-0
3-chloro-4-dimethoxymethyl-2-trifluoromethanesulfonyloxybenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / methanol / Reflux

2: sodium acetate / palladium diacetate; (diphenylphosphin)ferrocene / 4 h / 90 - 100 °C / 6375.64 Torr / Autoclave

3: triethylamine / dichloromethane / 20 °C / Cooling with ice

With sodium acetate; triethylamine; hydrogenchloride; (diphenylphosphin)ferrocene; palladium diacetate; In methanol; dichloromethane;