4-tert-butyl-1-methylcyclohexanol methyl ether

Base Information

• Chemical Name: 4-tert-butyl-1-methylcyclohexanol methyl ether
• CAS No.: 343853-71-4
• Molecular Formula: C₁₂H₂₄O
• Molecular Weight: 184.322
• Mol file: 343853-71-4.mol

Synonyms:4-tert-butyl-1-methylcyclohexanol methyl ether

Chemical Property of 4-tert-butyl-1-methylcyclohexanol methyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-tert-butyl-1-methylcyclohexanol methyl ether

There total 4 articles about 4-tert-butyl-1-methylcyclohexanol methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.8%

4-tert-butyl-1-methylcyclohexanol (6353-54-4) + methyl iodide (74-88-4) → 4-tert-butyl-1-methylcyclohexanol methyl ether (343853-71-4)

Guidance literature:

4-tert-butyl-1-methylcyclohexanol; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 5h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; mineral oil; at 20 ℃; for 2.5h;

Reference yield:

4-tercbutyl-cyclohexanone (98-53-3) → 4-tert-butyl-1-methylcyclohexanol methyl ether (343853-71-4)

Guidance literature:

Multi-step reaction with 2 steps

2: sodium hydride / diethyl ether / Heating

With sodium hydride; In diethyl ether;

DOI:10.1039/P19810001671

Reference yield:

cis-4-tert-butyl-1-methylcyclohexanol (16980-56-6) + methyl iodide (74-88-4) → 4-tert-butyl-1-methylcyclohexanol methyl ether (343853-71-4)

Guidance literature:

With sodium hydride; In diethyl ether; Heating;

DOI:10.1039/P19810001671

upstream raw materials:

cis-4-tert-butyl-1-methylcyclohexanol

methyl iodide

trans-4-tert-butyl-1-methylcyclohexanol

4-tercbutyl-cyclohexanone

Downstream raw materials:

4-tert-butyl-1-methylcyclohexanol