2-(8-methyl-6-phenyldipyrazolo[3,4-b:3',4'-d]pyridin-1(6H)-yl)-N-phenylacetamide

Base Information

Chemical Name:2-(8-methyl-6-phenyldipyrazolo[3,4-b:3',4'-d]pyridin-1(6H)-yl)-N-phenylacetamide
CAS No.:1263104-18-2
Molecular Formula:C₂₂H₁₈N₆O
Molecular Weight:382.425
Hs Code.:

Synonyms:2-(8-methyl-6-phenyldipyrazolo[3,4-b:3',4'-d]pyridin-1(6H)-yl)-N-phenylacetamide

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Chemical Property of 2-(8-methyl-6-phenyldipyrazolo[3,4-b:3',4'-d]pyridin-1(6H)-yl)-N-phenylacetamide

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Technology Process of 2-(8-methyl-6-phenyldipyrazolo[3,4-b:3',4'-d]pyridin-1(6H)-yl)-N-phenylacetamide

There total 3 articles about 2-(8-methyl-6-phenyldipyrazolo[3,4-b:3',4'-d]pyridin-1(6H)-yl)-N-phenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.66%

: 1263104-14-8
8-methyl-6-phenyl-1,6-dihydrodipyrazolo[3,4-b:3',4'-d]pyridine

: 5326-87-4
N-(phenyl)bromoacetamide

: 1263104-18-2
2-(8-methyl-6-phenyldipyrazolo[3,4-b:3',4'-d]pyridin-1(6H)-yl)-N-phenylacetamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 55 - 60 ℃; for 6h;
DOI:10.1007/s10895-010-0622-4

Reference yield:

: 1263104-04-6
(4-chloro-3-methyl-1-phenyl-1H-pyrazolo[3,4-b]pyridin-5-yl)methanone

: 1263104-18-2
2-(8-methyl-6-phenyldipyrazolo[3,4-b:3',4'-d]pyridin-1(6H)-yl)-N-phenylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / ethanol / 8 h / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 6 h / 55 - 60 °C

With potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1007/s10895-010-0622-4

Reference yield:

: 81153-44-8
4-chloro-3-methyl-1-phenyl-1H-pyrazolo[3,4-b]pyridine-5-carboxylic acid ethyl ester

: 1263104-18-2
2-(8-methyl-6-phenyldipyrazolo[3,4-b:3',4'-d]pyridin-1(6H)-yl)-N-phenylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / dichloromethane; toluene / 2 h / -78 °C

2: potassium carbonate / ethanol / 8 h / Reflux

3: potassium carbonate / N,N-dimethyl-formamide / 6 h / 55 - 60 °C

With diisobutylaluminium hydride; potassium carbonate; In ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1007/s10895-010-0622-4