C₅₃H₈₄N₆O₁₃

Base Information

Chemical Name:C₅₃H₈₄N₆O₁₃
CAS No.:1173157-86-2
Molecular Formula:C₅₃H₈₄N₆O₁₃
Molecular Weight:1013.28
Hs Code.:

C<sub>53</sub>H<sub>84</sub>N<sub>6</sub>O<sub>13</sub>

Synonyms:C₅₃H₈₄N₆O₁₃

Suppliers and Price of C₅₃H₈₄N₆O₁₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₃H₈₄N₆O₁₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₃H₈₄N₆O₁₃

There total 11 articles about C₅₃H₈₄N₆O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1173157-81-7
(2S)-N-{[4-(aminomethyl)phenyl]methoxy}-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide formic acid salt

: 174267-71-1
3,9-Bis(tert-butoxycarbonylmethyl)-6-carboxymethyl-3,6,9-triazaundecanedioic acid-di-tert-butyl ester

: 1173157-86-2
C₅₃H₈₄N₆O₁₃

Guidance literature:: 3,9-Bis(tert-butoxycarbonylmethyl)-6-carboxymethyl-3,6,9-triazaundecanedioic acid-di-tert-butyl ester; With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 22 ℃; for 0.25h;

(2S)-N-{[4-(aminomethyl)phenyl]methoxy}-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide formic acid salt; In N,N-dimethyl-formamide; for 0.5h;

Reference yield:

: 82732-07-8,108524-68-1,142926-43-0,100564-78-1
Boc-L-homophenylalanine

: 1173157-86-2
C₅₃H₈₄N₆O₁₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: methanol / dichloromethane; diethyl ether / 0.5 h / 22 °C

2.1: hydroxylamine hydrochloride; potassium hydroxide / methanol / 0 - 22 °C

3.1: potassium carbonate / ethanol; water / 1 h / 22 °C

4.1: diethylamine / trisodium tris(3-sulfophenyl)phosphine; palladium diacetate / acetonitrile; water / 1 h / 22 °C

5.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.25 h / 22 °C

5.2: 0.5 h

With methanol; hydroxylamine hydrochloride; potassium carbonate; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; diethylamine; N-ethyl-N,N-diisopropylamine; potassium hydroxide; trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; In methanol; diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 943-73-7
D-homophenylalanine

: 1173157-86-2
C₅₃H₈₄N₆O₁₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium carbonate / water; tetrahydrofuran / 1 h / 22 °C

1.2: pH 3 - 4

2.1: methanol / dichloromethane; diethyl ether / 0.5 h / 22 °C

3.1: hydroxylamine hydrochloride; potassium hydroxide / methanol / 0 - 22 °C

4.1: potassium carbonate / ethanol; water / 1 h / 22 °C

5.1: diethylamine / trisodium tris(3-sulfophenyl)phosphine; palladium diacetate / acetonitrile; water / 1 h / 22 °C

6.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.25 h / 22 °C

6.2: 0.5 h

With methanol; hydroxylamine hydrochloride; sodium carbonate; potassium carbonate; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; diethylamine; N-ethyl-N,N-diisopropylamine; potassium hydroxide; trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;