(Z)-Se-(3,5-dinitrobenzyl)-N-cyano-N,N'-di(4-methoxyphenyl)isoselenourea

Base Information

• Chemical Name: (Z)-Se-(3,5-dinitrobenzyl)-N-cyano-N,N'-di(4-methoxyphenyl)isoselenourea
• CAS No.: 1453815-65-0
• Molecular Formula: C₂₃H₁₉N₅O₆Se
• Molecular Weight: 540.394

Synonyms:(Z)-Se-(3,5-dinitrobenzyl)-N-cyano-N,N'-di(4-methoxyphenyl)isoselenourea

Chemical Property of (Z)-Se-(3,5-dinitrobenzyl)-N-cyano-N,N'-di(4-methoxyphenyl)isoselenourea

Chemical Property:

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Technology Process of (Z)-Se-(3,5-dinitrobenzyl)-N-cyano-N,N'-di(4-methoxyphenyl)isoselenourea

There total 3 articles about (Z)-Se-(3,5-dinitrobenzyl)-N-cyano-N,N'-di(4-methoxyphenyl)isoselenourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

4-methoxyphenyl isoselenocyanate (14223-47-3) + 3,5-dinitrobenzyl chloride (74367-78-5) → 5-[(3,5-Dinitrobenzyl)selanyl]-1-(4-methoxyphenyl)-1H-tetrazole (1453815-63-8) + N-(3,5-dinitrobenzyl)-N-(4-methoxyphenyl)cyanamide (1453815-64-9) + (Z)-Se-(3,5-dinitrobenzyl)-N-cyano-N,N'-di(4-methoxyphenyl)isoselenourea (1453815-65-0)

Guidance literature:

With sodium azide; In tetrahydrofuran; water;

DOI:10.1016/j.tet.2013.07.103

Reference yield: 19.0%

4-methoxyphenyl isoselenocyanate (14223-47-3) + 3,5-dinitrobenzyl iodide (192137-08-9) → 5-[(3,5-Dinitrobenzyl)selanyl]-1-(4-methoxyphenyl)-1H-tetrazole (1453815-63-8) + N-(3,5-dinitrobenzyl)-N-(4-methoxyphenyl)cyanamide (1453815-64-9) + (Z)-Se-(3,5-dinitrobenzyl)-N-cyano-N,N'-di(4-methoxyphenyl)isoselenourea (1453815-65-0)

Guidance literature:

With sodium azide; In tetrahydrofuran; water;

DOI:10.1016/j.tet.2013.07.103

Reference yield: 16.0%

4-methoxyphenyl isoselenocyanate (14223-47-3) + 3,5-dinitrobenzyl iodide (192137-08-9) → N-(3,5-dinitrobenzyl)-N-(4-methoxyphenyl)cyanamide (1453815-64-9) + (Z)-Se-(3,5-dinitrobenzyl)-N-cyano-N,N'-di(4-methoxyphenyl)isoselenourea (1453815-65-0)

Guidance literature:

With sodium azide; tetrabutylammomium bromide; In dichloromethane; water; at 20 ℃;

DOI:10.1016/j.tet.2013.07.103

upstream raw materials:

4-methoxyphenyl isoselenocyanate

3,5-dinitrobenzyl chloride

3,5-dinitrobenzyl iodide

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