6-bromo-2-(2,6-diisopropylphenyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione

Base Information

• Chemical Name: 6-bromo-2-(2,6-diisopropylphenyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione
• CAS No.: 187536-93-2
• Molecular Formula: C₂₄H₂₂BrNO₂
• Molecular Weight: 436.348

Synonyms:6-bromo-2-(2,6-diisopropylphenyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione

Chemical Property of 6-bromo-2-(2,6-diisopropylphenyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione

Chemical Property:

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Technology Process of 6-bromo-2-(2,6-diisopropylphenyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione

There total 2 articles about 6-bromo-2-(2,6-diisopropylphenyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

4-bromo-1,8-naphthalenedicarboxylic anhydride (81-86-7) + 2,6-diisopropylbenzenamine (24544-04-5) → 6-bromo-2-(2,6-diisopropylphenyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione (187536-93-2)

Guidance literature:

With propionic acid; at 150 ℃; for 17h; Inert atmosphere;

DOI:10.1021/jacs.7b09459

Reference yield: 80.0%

4-bromo-1,8-naphthalenedicarboxylic anhydride (81-86-7) + diisopropylamine (108-18-9) → 6-bromo-2-(2,6-diisopropylphenyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione (187536-93-2)

Guidance literature:

In acetic acid; for 6h; under 760.051 Torr; Reflux; Microwave irradiation;

DOI:10.1039/c3cc44590a

Reference yield: 96.0%

4-chloro-phenol (106-48-9,82344-39-6) + 6-bromo-2-(2,6-diisopropylphenyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione (187536-93-2) → 4-(4-chlorophenoxy)-N-(2',6'-diisopropylphenyl)-1,8-naphthalimide (1616788-67-0)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 12h;

DOI:10.1016/j.dyepig.2014.05.007

upstream raw materials:

4-bromo-1,8-naphthalenedicarboxylic anhydride

2,6-diisopropylbenzenamine

diisopropylamine

Downstream raw materials:

N-(2,6-diisopropylphenyl)-9-(4-N-(2,6-diisopropylphenyl)naphthalene-1,8-dicarboximide)perylene-3,4-dicarboximide

N,N’-bis(2,6-diisopropylphenyl)-terrylene-3,4,11,12-tetracarboximide

N-(2,6-diisopropylphenyl)-4-((p-cyanophenyl)amino)naphthalene-1,8-dicarboximide

2-(2,6-diisopropylphenyl)-6-(isoquinolin-8-yl)-1H-benzo[de]isoquinoline-1,3(2H)-dione

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