3-benzyloxy-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

Base Information

Chemical Name:3-benzyloxy-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester
CAS No.:114476-15-2
Molecular Formula:C₂₄H₂₆N₂O₄
Molecular Weight:406.481
Hs Code.:

Synonyms:3-benzyloxy-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

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Chemical Property of 3-benzyloxy-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

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Technology Process of 3-benzyloxy-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

There total 11 articles about 3-benzyloxy-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 67-56-1
methanol

: 114476-26-5
3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaureamid

: 114476-15-2
3-benzyloxy-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

Guidance literature:: With Amberlyst 15; at 60 ℃;
DOI:10.1016/S0040-4020(01)86861-7

Reference yield:

: 885-40-5
(+/-)-harmacine

: 114476-15-2
3-benzyloxy-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

Guidance literature:: Multi-step reaction with 3 steps

1: 44 percent / tetrahydrofuran; acetone / 1 h / Ambient temperature; Heating

2: 76 percent / sodium hydroxide, 30percent hydrogen peroxide / CH₂Cl₂; ethanol / 48 h

3: 53 percent / amberlyst 15 / 60 °C

With sodium hydroxide; Amberlyst 15; dihydrogen peroxide; In tetrahydrofuran; ethanol; dichloromethane; acetone;
DOI:10.1016/S0040-4020(01)86861-7

Reference yield:

: 114476-07-2
3-cyan-1,2,3,4,5,6,7,8-octahydoazonino<5,4-b>indol-7-carbonitril

: 114476-15-2
3-benzyloxy-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

Guidance literature:: Multi-step reaction with 5 steps

1: 71 percent / potassium hydroxide / 0.42 h / Heating

2: 64 percent / 80 percent acetic acid / 60 h / Heating

3: 44 percent / tetrahydrofuran; acetone / 1 h / Ambient temperature; Heating

4: 76 percent / sodium hydroxide, 30percent hydrogen peroxide / CH₂Cl₂; ethanol / 48 h

5: 53 percent / amberlyst 15 / 60 °C

With potassium hydroxide; sodium hydroxide; Amberlyst 15; dihydrogen peroxide; acetic acid; In tetrahydrofuran; ethanol; dichloromethane; acetone;
DOI:10.1016/S0040-4020(01)86861-7