ethyl 2-bromo-2-cyclohexenyl carbonate

Base Information

Chemical Name:ethyl 2-bromo-2-cyclohexenyl carbonate
CAS No.:97861-66-0
Molecular Formula:C₉H₁₃BrO₃
Molecular Weight:249.104
Hs Code.:

Synonyms:ethyl 2-bromo-2-cyclohexenyl carbonate

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Chemical Property of ethyl 2-bromo-2-cyclohexenyl carbonate

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Technology Process of ethyl 2-bromo-2-cyclohexenyl carbonate

There total 2 articles about ethyl 2-bromo-2-cyclohexenyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 109380-07-6,109431-74-5,122797-27-7,61426-49-1
2-bromocyclohex-2-en-1-ol

: 541-41-3
chloroformic acid ethyl ester

: 97861-66-0
ethyl 2-bromo-2-cyclohexenyl carbonate

Guidance literature:: With pyridine; In diethyl ether; for 12h;
DOI:10.1021/jo00220a043

Reference yield:

: 14310-04-4
2-bromocyclohex-2-en-1-yl acetate

: 97861-66-0
ethyl 2-bromo-2-cyclohexenyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / (PPh₃)2PdCl₂ / 2 h / 80 °C / var. 2-bromoallyl acetates, other secondary and tertiary cyclic amines

2: 78 percent / pyridine / diethyl ether / 12 h

With pyridine; bis-triphenylphosphine-palladium(II) chloride; In diethyl ether;
DOI:10.1021/jo00220a043