diethyl 2-((tert-butoxycarbonyl)amino)-2-(16-(tosyloxy)hexadecyl)malonate

Base Information

Chemical Name:diethyl 2-((tert-butoxycarbonyl)amino)-2-(16-(tosyloxy)hexadecyl)malonate
CAS No.:1426083-80-8
Molecular Formula:C₃₅H₅₉NO₉S
Molecular Weight:669.921
Hs Code.:

Synonyms:diethyl 2-((tert-butoxycarbonyl)amino)-2-(16-(tosyloxy)hexadecyl)malonate

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Chemical Property of diethyl 2-((tert-butoxycarbonyl)amino)-2-(16-(tosyloxy)hexadecyl)malonate

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Technology Process of diethyl 2-((tert-butoxycarbonyl)amino)-2-(16-(tosyloxy)hexadecyl)malonate

There total 8 articles about diethyl 2-((tert-butoxycarbonyl)amino)-2-(16-(tosyloxy)hexadecyl)malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 1426083-79-5
diethyl 2-[(tert-butoxycarbonyl)amino]-2-(16-hydroxyhexadecyl)malonate

: 98-59-9
p-toluenesulfonyl chloride

: 1426083-80-8
diethyl 2-((tert-butoxycarbonyl)amino)-2-(16-(tosyloxy)hexadecyl)malonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 59101-28-9
16-bromohexadecan-1-ol

: 1426083-80-8
diethyl 2-((tert-butoxycarbonyl)amino)-2-(16-(tosyloxy)hexadecyl)malonate

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / acetonitrile / 6 h / Reflux

2: triethylamine / dichloromethane; water / 0 - 20 °C

With caesium carbonate; triethylamine; In dichloromethane; water; acetonitrile;

Reference yield:

: 102831-44-7
diethyl tert-butoxycarbonylaminomalonate

: 1426083-80-8
diethyl 2-((tert-butoxycarbonyl)amino)-2-(16-(tosyloxy)hexadecyl)malonate

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / acetonitrile / 6 h / Reflux

2: triethylamine / dichloromethane; water / 0 - 20 °C

With caesium carbonate; triethylamine; In dichloromethane; water; acetonitrile;