17-[(tert-butoxycarbonyl)amino]-18-hydroxy-17-(hydroxymethyl)octadecyl 4-methylbenzenesulfonate

Base Information

Chemical Name:17-[(tert-butoxycarbonyl)amino]-18-hydroxy-17-(hydroxymethyl)octadecyl 4-methylbenzenesulfonate
CAS No.:1426083-81-9
Molecular Formula:C₃₁H₅₅NO₇S
Molecular Weight:585.846
Hs Code.:

Synonyms:17-[(tert-butoxycarbonyl)amino]-18-hydroxy-17-(hydroxymethyl)octadecyl 4-methylbenzenesulfonate

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Chemical Property of 17-[(tert-butoxycarbonyl)amino]-18-hydroxy-17-(hydroxymethyl)octadecyl 4-methylbenzenesulfonate

Chemical Property:

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Technology Process of 17-[(tert-butoxycarbonyl)amino]-18-hydroxy-17-(hydroxymethyl)octadecyl 4-methylbenzenesulfonate

There total 7 articles about 17-[(tert-butoxycarbonyl)amino]-18-hydroxy-17-(hydroxymethyl)octadecyl 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59101-28-9
16-bromohexadecan-1-ol

: 1426083-81-9
17-[(tert-butoxycarbonyl)amino]-18-hydroxy-17-(hydroxymethyl)octadecyl 4-methylbenzenesulfonate

: 1426083-82-0
C₃₀H₅₃NO₆S

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / acetonitrile / 6 h / Reflux

2: triethylamine / dichloromethane; water / 0 - 20 °C

3: lithium borohydride / tetrahydrofuran / 0 - 20 °C

With lithium borohydride; caesium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; water; acetonitrile;

Reference yield:

: 1426083-80-8
diethyl 2-((tert-butoxycarbonyl)amino)-2-(16-(tosyloxy)hexadecyl)malonate

: 1426083-81-9
17-[(tert-butoxycarbonyl)amino]-18-hydroxy-17-(hydroxymethyl)octadecyl 4-methylbenzenesulfonate

: 1426083-82-0
C₃₀H₅₃NO₆S

Guidance literature:: With lithium borohydride; In tetrahydrofuran; at 0 - 20 ℃;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1426083-81-9
17-[(tert-butoxycarbonyl)amino]-18-hydroxy-17-(hydroxymethyl)octadecyl 4-methylbenzenesulfonate

: 1426083-82-0
C₃₀H₅₃NO₆S

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / 1,4-dioxane / 24 h / 5 - 20 °C

2: caesium carbonate / acetonitrile / 6 h / Reflux

3: triethylamine / dichloromethane; water / 0 - 20 °C

4: lithium borohydride / tetrahydrofuran / 0 - 20 °C

With lithium borohydride; caesium carbonate; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; acetonitrile;