17-amino-18-hydroxy-17-(hydroxymethyl)octadecyl 4-methylbenzenesulfonate

Base Information

Chemical Name:17-amino-18-hydroxy-17-(hydroxymethyl)octadecyl 4-methylbenzenesulfonate
CAS No.:1426083-83-1
Molecular Formula:C₂₆H₄₇NO₅S
Molecular Weight:485.729
Hs Code.:

Synonyms:17-amino-18-hydroxy-17-(hydroxymethyl)octadecyl 4-methylbenzenesulfonate

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Chemical Property of 17-amino-18-hydroxy-17-(hydroxymethyl)octadecyl 4-methylbenzenesulfonate

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Technology Process of 17-amino-18-hydroxy-17-(hydroxymethyl)octadecyl 4-methylbenzenesulfonate

There total 6 articles about 17-amino-18-hydroxy-17-(hydroxymethyl)octadecyl 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1426083-81-9
17-[(tert-butoxycarbonyl)amino]-18-hydroxy-17-(hydroxymethyl)octadecyl 4-methylbenzenesulfonate

: 1426083-83-1
17-amino-18-hydroxy-17-(hydroxymethyl)octadecyl 4-methylbenzenesulfonate

Guidance literature:: With hydrogenchloride; In water; ethyl acetate; at 20 ℃; for 120h;

Reference yield:

: 59101-28-9
16-bromohexadecan-1-ol

: 1426083-83-1
17-amino-18-hydroxy-17-(hydroxymethyl)octadecyl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: caesium carbonate / acetonitrile / 6 h / Reflux

2: triethylamine / dichloromethane; water / 0 - 20 °C

3: lithium borohydride / tetrahydrofuran / 0 - 20 °C

4: hydrogenchloride / ethyl acetate; water / 120 h / 20 °C

With hydrogenchloride; lithium borohydride; caesium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; water; ethyl acetate; acetonitrile;

Reference yield:

: 1426083-79-5
diethyl 2-[(tert-butoxycarbonyl)amino]-2-(16-hydroxyhexadecyl)malonate

: 1426083-83-1
17-amino-18-hydroxy-17-(hydroxymethyl)octadecyl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane; water / 0 - 20 °C

2: lithium borohydride / tetrahydrofuran / 0 - 20 °C

3: hydrogenchloride / ethyl acetate; water / 120 h / 20 °C

With hydrogenchloride; lithium borohydride; triethylamine; In tetrahydrofuran; dichloromethane; water; ethyl acetate;