1-(3-nitrophenyl)-5-phenyl-N³,N⁴-di-m-tolyl-1H-pyrazole-3,4-dicarboxamide

Base Information

Chemical Name:1-(3-nitrophenyl)-5-phenyl-N³,N⁴-di-m-tolyl-1H-pyrazole-3,4-dicarboxamide
CAS No.:1608108-02-6
Molecular Formula:C₃₁H₂₅N₅O₄
Molecular Weight:531.571
Hs Code.:

1-(3-nitrophenyl)-5-phenyl-N<sup>3</sup>,N<sup>4</sup>-di-m-tolyl-1H-pyrazole-3,4-dicarboxamide

Synonyms:1-(3-nitrophenyl)-5-phenyl-N³,N⁴-di-m-tolyl-1H-pyrazole-3,4-dicarboxamide

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Chemical Property of 1-(3-nitrophenyl)-5-phenyl-N³,N⁴-di-m-tolyl-1H-pyrazole-3,4-dicarboxamide

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Technology Process of 1-(3-nitrophenyl)-5-phenyl-N³,N⁴-di-m-tolyl-1H-pyrazole-3,4-dicarboxamide

There total 3 articles about 1-(3-nitrophenyl)-5-phenyl-N³,N⁴-di-m-tolyl-1H-pyrazole-3,4-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1608107-87-4
1-(3-nitrophenyl)-5-phenyl-1H-pyrazole-3,4-dicarbonyl dichloride

: 108-44-1
1-amino-3-methylbenzene

: 1608108-02-6
1-(3-nitrophenyl)-5-phenyl-N³,N⁴-di-m-tolyl-1H-pyrazole-3,4-dicarboxamide

Guidance literature:: In 5,5-dimethyl-1,3-cyclohexadiene; at 140 ℃; for 3h;
DOI:10.1016/j.ejmech.2014.03.033

Reference yield:

: 96723-10-3
1-(3-nitrophenyl)-5-phenyl-1H-pyrazole-3,4-dicarboxylic acid

: 1608108-02-6
1-(3-nitrophenyl)-5-phenyl-N³,N⁴-di-m-tolyl-1H-pyrazole-3,4-dicarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 5 h / 80 °C

2: 5,5-dimethyl-1,3-cyclohexadiene / 3 h / 140 °C

With thionyl chloride; In 5,5-dimethyl-1,3-cyclohexadiene;
DOI:10.1016/j.ejmech.2014.03.033

Reference yield:

: 1152334-07-0
4-(ethoxycarbonyl)-1-(3-nitrophenyl)-5-phenyl-1H-pyrazole-3-carboxylic acid

: 1608108-02-6
1-(3-nitrophenyl)-5-phenyl-N³,N⁴-di-m-tolyl-1H-pyrazole-3,4-dicarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / water / 3 h / 100 °C

2: thionyl chloride / 5 h / 80 °C

3: 5,5-dimethyl-1,3-cyclohexadiene / 3 h / 140 °C

With thionyl chloride; sodium hydroxide; In 5,5-dimethyl-1,3-cyclohexadiene; water;
DOI:10.1016/j.ejmech.2014.03.033