Technology Process of C42H46N4O12
There total 8 articles about C42H46N4O12 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 98 percent / imidazole / tetrahydrofuran
2: 89 percent / acetic acid; water
3: NBS; 2,6-lutidine; 4 Angstroem molecular sieve / CH2Cl2
4: acetic acid; water
5: 30 percent / H2O; acetonitrile / UV-irradiation
6: 55 percent / pyridine
7: 70 percent / TBAF / tetrahydrofuran
With
pyridine; 1H-imidazole; 2,6-dimethylpyridine; N-Bromosuccinimide; 4 A molecular sieve; tetrabutyl ammonium fluoride; water; acetic acid;
In
tetrahydrofuran; dichloromethane; water; acetonitrile;
1: silylation / 2: Hydrolysis / 3: Condensation / 4: Hydrolysis / 5: Cyclization / 6: Substitution / 7: desilylation;
DOI:10.1016/S0040-4039(00)00127-1
- Guidance literature:
-
Multi-step reaction with 5 steps
1: NBS; 2,6-lutidine; 4 Angstroem molecular sieve / CH2Cl2
2: acetic acid; water
3: 30 percent / H2O; acetonitrile / UV-irradiation
4: 55 percent / pyridine
5: 70 percent / TBAF / tetrahydrofuran
With
pyridine; 2,6-dimethylpyridine; N-Bromosuccinimide; 4 A molecular sieve; tetrabutyl ammonium fluoride; water; acetic acid;
In
tetrahydrofuran; dichloromethane; water; acetonitrile;
1: Condensation / 2: Hydrolysis / 3: Cyclization / 4: Substitution / 5: desilylation;
DOI:10.1016/S0040-4039(00)00127-1