10-(4-(trifluoromethyl)benzyl)-2-methoxyphenanthrene

Base Information

Chemical Name:10-(4-(trifluoromethyl)benzyl)-2-methoxyphenanthrene
CAS No.:1332500-55-6
Molecular Formula:C₂₃H₁₇F₃O
Molecular Weight:366.383
Hs Code.:

Synonyms:10-(4-(trifluoromethyl)benzyl)-2-methoxyphenanthrene

Suppliers and Price of 10-(4-(trifluoromethyl)benzyl)-2-methoxyphenanthrene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 10-(4-(trifluoromethyl)benzyl)-2-methoxyphenanthrene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 10-(4-(trifluoromethyl)benzyl)-2-methoxyphenanthrene

There total 3 articles about 10-(4-(trifluoromethyl)benzyl)-2-methoxyphenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1332500-49-8
N'-((4'-methoxybiphenyl-2-yl)methylene)-4-methylbenzenesulfonohydrazide

: 705-31-7
4-trifluoromethylphenylacetylene

: 1332500-55-6
10-(4-(trifluoromethyl)benzyl)-2-methoxyphenanthrene

Guidance literature:: With tetrabutylammomium bromide; copper(ll) bromide; lithium tert-butoxide; In 1,4-dioxane; at 90 - 120 ℃; for 28h; Inert atmosphere;
DOI:10.1021/ol201788v

Reference yield:

: 5720-07-0
4-methoxyphenylboronic acid

: 1332500-55-6
10-(4-(trifluoromethyl)benzyl)-2-methoxyphenanthrene

Guidance literature:: Multi-step reaction with 3 steps

1: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / water; N,N-dimethyl-formamide / 12 h / 110 °C / Inert atmosphere

2: methanol / 60 °C / Inert atmosphere

3: tetrabutylammomium bromide; copper(ll) bromide; lithium tert-butoxide / 1,4-dioxane / 28 h / 90 - 120 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; tetrabutylammomium bromide; potassium carbonate; copper(ll) bromide; lithium tert-butoxide; In 1,4-dioxane; methanol; water; N,N-dimethyl-formamide; 1: Suzuki coupling;
DOI:10.1021/ol201788v

Reference yield:

: 16064-04-3
2-(4-methoxyphenyl)benzaldehyde

: 1332500-55-6
10-(4-(trifluoromethyl)benzyl)-2-methoxyphenanthrene

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 60 °C / Inert atmosphere

2: tetrabutylammomium bromide; copper(ll) bromide; lithium tert-butoxide / 1,4-dioxane / 28 h / 90 - 120 °C / Inert atmosphere

With tetrabutylammomium bromide; copper(ll) bromide; lithium tert-butoxide; In 1,4-dioxane; methanol;
DOI:10.1021/ol201788v