N'-((4'-methoxybiphenyl-2-yl)methylene)-4-methylbenzenesulfonohydrazide

Base Information

Chemical Name:N'-((4'-methoxybiphenyl-2-yl)methylene)-4-methylbenzenesulfonohydrazide
CAS No.:1332500-49-8
Molecular Formula:C₂₁H₂₀N₂O₃S
Molecular Weight:380.467
Hs Code.:

Synonyms:N'-((4'-methoxybiphenyl-2-yl)methylene)-4-methylbenzenesulfonohydrazide

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Chemical Property of N'-((4'-methoxybiphenyl-2-yl)methylene)-4-methylbenzenesulfonohydrazide

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Technology Process of N'-((4'-methoxybiphenyl-2-yl)methylene)-4-methylbenzenesulfonohydrazide

There total 2 articles about N'-((4'-methoxybiphenyl-2-yl)methylene)-4-methylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 16064-04-3
2-(4-methoxyphenyl)benzaldehyde

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1332500-49-8
N'-((4'-methoxybiphenyl-2-yl)methylene)-4-methylbenzenesulfonohydrazide

Guidance literature:: In methanol; at 60 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1021/jo501489c

Reference yield:

: 5720-07-0
4-methoxyphenylboronic acid

: 1332500-49-8
N'-((4'-methoxybiphenyl-2-yl)methylene)-4-methylbenzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / water; N,N-dimethyl-formamide / 12 h / 110 °C / Inert atmosphere

2: methanol / 60 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; In methanol; water; N,N-dimethyl-formamide; 1: Suzuki coupling;
DOI:10.1021/ol201788v

Reference yield: 68.0%

: 766-98-3
1-ethynyl-4-fluorobenzene

: 1332500-49-8
N'-((4'-methoxybiphenyl-2-yl)methylene)-4-methylbenzenesulfonohydrazide

: 1332500-57-8
10-(4-fluorobenzyl)-2-methoxyphenanthrene

Guidance literature:: With tetrabutylammomium bromide; copper(ll) bromide; lithium tert-butoxide; In 1,4-dioxane; at 90 - 120 ℃; for 28h; Inert atmosphere;
DOI:10.1021/ol201788v