3-(4-nitrophenyl)-1-phthalimidospiro[aziridine-2,2’-indene]-1’,3’-dione

Base Information

• Chemical Name: 3-(4-nitrophenyl)-1-phthalimidospiro[aziridine-2,2’-indene]-1’,3’-dione
• CAS No.: 1207272-26-1
• Molecular Formula: C₂₄H₁₃N₃O₆
• Molecular Weight: 439.384

Synonyms:3-(4-nitrophenyl)-1-phthalimidospiro[aziridine-2,2’-indene]-1’,3’-dione

Chemical Property of 3-(4-nitrophenyl)-1-phthalimidospiro[aziridine-2,2’-indene]-1’,3’-dione

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Technology Process of 3-(4-nitrophenyl)-1-phthalimidospiro[aziridine-2,2’-indene]-1’,3’-dione

There total 1 articles about 3-(4-nitrophenyl)-1-phthalimidospiro[aziridine-2,2’-indene]-1’,3’-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

2-(p-nitrobenzylidene)indan-1,3-dione (15875-60-2) + N-aminophthalamide (1875-48-5) → 3-(4-nitrophenyl)-1-phthalimidospiro[aziridine-2,2’-indene]-1’,3’-dione (1207272-26-1)

Guidance literature:

With lead(IV) tetraacetate; potassium carbonate; In dichloromethane; at 0 ℃; for 0.5h;

DOI:10.1016/j.tetlet.2014.03.014

Reference yield: 66.0%

3-(4-nitrophenyl)-1-phthalimidospiro[aziridine-2,2’-indene]-1’,3’-dione (1207272-26-1) + dimethyl acetylenedicarboxylate (762-42-5) → 2-(4-nitrophenyl)-4H-indeno[2,1-d][1,3]oxazol-4-one (1207272-27-2) + dimethyl 5'-(4-nitrophenyl)-1,3-dioxo-1'-phthalimido-1,1',3,5'-tetrahydrospiro[indene-2,2'-pyrrole]-3',4'-dicarboxylate (1600516-55-9)

Guidance literature:

In benzene; at 75 ℃; for 8h;

DOI:10.1016/j.tetlet.2014.03.014

Reference yield: 60.0%

3-(4-nitrophenyl)-1-phthalimidospiro[aziridine-2,2’-indene]-1’,3’-dione (1207272-26-1) → 2-(4-nitrophenyl)-4H-indeno[2,1-d][1,3]oxazol-4-one (1207272-27-2)

Guidance literature:

With dimethylfumarate; In benzene; at 75 ℃; for 8h;

DOI:10.1016/j.tetlet.2014.03.014

upstream raw materials:

2-(p-nitrobenzylidene)indan-1,3-dione

N-aminophthalamide

Downstream raw materials:

2-(4-nitrophenyl)-4H-indeno[2,1-d][1,3]oxazol-4-one

dimethyl 5'-(4-nitrophenyl)-1,3-dioxo-1'-phthalimido-1,1',3,5'-tetrahydrospiro[indene-2,2'-pyrrole]-3',4'-dicarboxylate

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