(E)-2-[3-(4-methoxyphenyl)prop-2-enoyl]phenyl nonafluorobutanesulfonate

Base Information

Chemical Name:(E)-2-[3-(4-methoxyphenyl)prop-2-enoyl]phenyl nonafluorobutanesulfonate
CAS No.:960505-52-6
Molecular Formula:C₂₀H₁₃F₉O₅S
Molecular Weight:536.372
Hs Code.:

Synonyms:(E)-2-[3-(4-methoxyphenyl)prop-2-enoyl]phenyl nonafluorobutanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-[3-(4-methoxyphenyl)prop-2-enoyl]phenyl nonafluorobutanesulfonate

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Technology Process of (E)-2-[3-(4-methoxyphenyl)prop-2-enoyl]phenyl nonafluorobutanesulfonate

There total 1 articles about (E)-2-[3-(4-methoxyphenyl)prop-2-enoyl]phenyl nonafluorobutanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 375-72-4
Nonafluorobutanesulfonyl fluoride

: 34000-29-8
[E]-3-(p-methoxyphenyl)-1-(2-hydroxyphenyl)prop-2-en-1-one

: 960505-52-6
(E)-2-[3-(4-methoxyphenyl)prop-2-enoyl]phenyl nonafluorobutanesulfonate

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo701741y

Reference yield:

: 960505-52-6
(E)-2-[3-(4-methoxyphenyl)prop-2-enoyl]phenyl nonafluorobutanesulfonate

: (R)-3-(4-methoxyphenyl)-2,3-dihydro-1H-inden-1-one

: (S)-3-(4-methoxyphenyl)-2,3-dihydro-1H-inden-1-one

Guidance literature:: With Proton Sponge; palladium diacetate; In N,N-dimethyl-formamide; at 100 ℃; for 12h; Title compound not separated from byproducts.;
DOI:10.1021/jo701741y

Reference yield:

: 79-55-0
1,2,2,6,6-pentamethylpiperidine

: 960505-52-6
(E)-2-[3-(4-methoxyphenyl)prop-2-enoyl]phenyl nonafluorobutanesulfonate

: (3R)-(4-methoxyphenyl)-2-methylene-indan-1-one

: (3S)-(4-methoxyphenyl)-2-methylene-indan-1-one

Guidance literature:: With (R)-3,5-XylMeOBIPHEP; palladium diacetate; In 1,4-dioxane; at 100 ℃; for 12h; Title compound not separated from byproducts.;
DOI:10.1021/jo701741y